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Porous titanium–silver dental implants fabricated via SPS: Poly-caprolactone coating and bioevaluation Cover

Porous titanium–silver dental implants fabricated via SPS: Poly-caprolactone coating and bioevaluation

Open Access
|Oct 2025

Abstract

Titanium implants are among the most widely used implants in dentistry; however, their use is associated with difficulties. Among the challenges in the construction and application of these implants, three important ones are considered in this study: (1) reducing construction temperature and time, (2) decreasing infection rate after implant loading, and (3) eliminating stress shielding. The first stage is making pieces of Ti–1 wt% Ag by spark plasma sintering at 850 and 900°C and pressure of 10 and 30 MPa. In the second stage, by sol–gel and immersion, poly-caprolactone was placed on the surface. For characterization, porosity, hardness, compressive strength, corrosion, and wettability were evaluated, and X-ray diffraction (XRD), scanning electron microscope (SEM), Fourier-transform infrared, field emission scanning electron microscopy, antibacterial test, and MTT were performed. XRD results indicated that the addition of 1% Ag to Ti did not change the crystalline phase. Also, Ag is completely dissolved in the structure of Ti and forms a substitutional solid solution. SEM results showed that samples made at 850°C and 10 MPa had 20–25% porosity. The average size of porosities is 5 μm with a morphology similar to interconnected spheres. Hardness and compressive tests showed that the best manufacturing conditions were 850°C and 10 MPa. After etching and coating, the samples have the highest wettability rate. Results of electrochemical tests showed that the corrosion potential of Ti–1 wt% Ag with coating is higher than the uncoated structure. In the cytotoxicity test, cell viability was improved by coating. Antibacterial test indicates that the coated sample is able to kill bacteria.

DOI: https://doi.org/10.2478/msp-2025-0030 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 85 - 105
Submitted on: May 8, 2025
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Accepted on: Aug 26, 2025
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Published on: Oct 3, 2025
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2025 Golsa Mousavi, Bijan Eftekhari Yekta, Jafar Javadpour, Hassan Saghafian, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.