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Insights into the multistep transformation of titanate nanotubes into nanowires and nanoribbons Cover

Insights into the multistep transformation of titanate nanotubes into nanowires and nanoribbons

Materials Science-Poland
Volume 34 (2016): Issue 4 (December 2016)
By: Agnieszka Baszczuk,  Marek Jasiorski,  Beata Borak and  Jerzy Wódka  
Open Access
|Nov 2016

Figures & Tables

TEM images of hydrothermal products synthesized at 120 °C for: (A) 24 h, (B) 72 h and (C) 120 h.
TEM images of hydrothermal products synthesized at 150 °C for: (A) 24 h and (B) 48 h.
Electron microscopy images (TEM and SEM) of hydrothermal products synthesized at 200 °C for: (A) 10 h and (B) 24 h.
XRD patterns of materials obtained after hydrothermal synthesis at 120 °C: (b) 24 h, (c) 72 h, (d) 120 h. The XRD pattern of TiO2 raw powder is given in (a) as reference.
Raman spectra of materials obtained after hydrothermal synthesis at 120 °C: (a) 24 h, (b) 72 h, (c) 120 h.
Comparison between the XRD patterns of the materials synthesized at 120 °C and 150 °C: (a) 120 °C, 120 h, (b) 150 °C, 24 h and (c) 150 °C 48 h.
Raman spectra of materials obtained after hydrothermal synthesis at 150 °C: (b) 24 h, (c) 48 h and as a reference Raman spectrum of material synthesized at 120 °C for 120 h (a).
XRD patterns of materials after hydrothermal synthesis at 200 °C: (b) 10 h, (c) 24 h and material after hydrothermal synthesis at 150 °C for 72 h (a). The XRD pattern of H2Ti3O7 generated using the data deposited in ICSD database by Gateshki et. al. [18] is given in (d) as reference.
Raman spectra of materials obtained after hydrothermal synthesis at 200 °C: (b) for 24 h, (c) for 10 h and as a reference Raman spectrum of material synthesized at 150 °C for 48 h (a).
DOI: https://doi.org/10.1515/msp-2016-0094 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 691 - 702
Submitted on: Aug 20, 2015
|
Accepted on: Jul 26, 2016
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Published on: Nov 17, 2016
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year
Keywords:
titanate nanotubes,
nanoribbons,
nanowires,
hydrothermal synthesis,
structure and morphology
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2016 Agnieszka Baszczuk, Marek Jasiorski, Beata Borak, Jerzy Wódka, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

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