Skip to main content
Have a personal or library account? Click to login
Crystal structure and spectroscopic properties of 4-acetaminopyridine and its protonated form Cover

Crystal structure and spectroscopic properties of 4-acetaminopyridine and its protonated form

Green Sciences
Volume 11 (2009): Issue 3 (September 2009)
By: ,  ,  ,  ,  ,   and    
Open Access
|Oct 2009
References

References

  1. Molgo, J., Lemeignan, M., Peradejordi, F. & Lechat, P. (1985). Presynaptic effects of aminopyridines on the neuromuscular junction of vertebrates16, 109-121.
    Search in Google Scholar
  2. Kirsch, G. E., Yeh, J. Z. & Oxford, G. S. (1986). Modulation of aminopyridine block of potassium currents in squid axon,50, 637-644.
    Search in Google Scholar
  3. Molgo, J., Lemeignan, M., Lechat, P. & Peradejordi, F. (1985). Increase in evoked transmitter release from motor nerve terminals by some amino N-heterocyclic compounds I. Comparative experimental activities and extracellular pH-dependence,20, 149-153.
    Search in Google Scholar
  4. Carlsson, C., Rosen, I. & Nilsson, E. (1993) Can 4-Aminopyridine be Used to Reverse Anaesthesia and Muscle Relaxation?, 27, 87-90.
    Search in Google Scholar
  5. Schwid, S., Petrie, M., McDermott, M., Tierney, D., Maso, D. & Goodman, A. (1997). Quantitative assessment of sustained-release 4-aminopyridine for symptomatic treatment of multiple sclerosis,48, 817-821.
    Open DOISearch in Google Scholar
  6. McEvoy, K. M., Windebank, A. J., Daube, J. R. & Low, P. A., (1989). 3,4-Diaminopyridine in the treatment of Lambert-Eaton myasthenic syndrome.321, 1567-1571.
    Open DOISearch in Google Scholar
  7. Segal, J. L. & Brunnemann, S. R. (1997). 4-Aminopyridine improves pulmonary function in quadriplegic humans with long-standing spinal cord injury.17, 415-423.
    Search in Google Scholar
  8. Sellin, L. C. (1981). The action of botulinum toxin at the neuromuscular junction.59, 11-20.
    Search in Google Scholar
  9. Davidson, M., Zemishlany, J. H. & Mohs, R. C. (1988). Alzheimer's Disease: A Report of Progress in Research.23, 485-490.
    Open DOISearch in Google Scholar
  10. Meves, H. & Pichon, H. (1979). The effects of 4-aminopyridine on the potassium current in internally profused giant axons of the squid.251, 60-63.
    Search in Google Scholar
  11. Raust, J., Goulay-Dufay, S., Le Hoang, M., Pradeau, D. & Guyon, F. (2007). Stability studies of ionised and nonionised 3,4-diaminopyridine: Hypothesis of degradation pathways and chemical structure of degradation products,43, 83-88.
    Open DOISearch in Google Scholar
  12. Ivanova, B. & Mayer-Figge, H. (2005). Crystal structure and Solid state IR-LD spectral analysis of new mononuclear Cu(II) complex with 4-aminopyridine.58, 653-659.
    Open DOISearch in Google Scholar
  13. Ivanova, B., Arnaudov, M. & Mayer-Figge, H. Molecular spectral analysis and crystal structure of 4-aminopyridinium tetrachloropalladate(II) complex salt. (2005).24(13), 1624-1630.
    Open DOISearch in Google Scholar
  14. Koleva, B., Trendafilova, E., Arnaudov, M., Sheldrick, W. S. & Mayer-Figge, H. (2006). Structural analysis of a mononuclear copper(II) complex of 3-aminopyridine.31, 866-873.
    Open DOISearch in Google Scholar
  15. Koleva, B. B., Kolev, T., Tsanev, T., Kotov, St., Mayer-Figge, H., Seidel, R. W. & Sheldrick, W. S. (2008). Spectroscopic and structural elucidation of 3,4-diaminopyridine and its hydrogentartarate salt. Crystal structure of 3,4-diaminopyridinium hydrogentartarate dehydrate.881, 146-155.
    Open DOISearch in Google Scholar
  16. Koleva, B. B., Kolev, T., Tsanev, T., Kotov, St., Mayer-Figge, H., Seidel, R. S. & Sheldrick, W. S. (2008). 3,4-diaminopyridine bis(perchlorate): structural and spectroscopic elucidation?19(1), 13-20.
    Search in Google Scholar
  17. Koleva, B. B., Kolev, T., Seidel, R. W., Tsanev, T., Mayer-Figge, H., Spiteller, M. & Sheldrick, W. S. (2008). Spectroscopic and structural elucidation of 4-dimethylaminopyridine and its hydrogensquarate., 71,. 695-702.
    Open DOISearch in Google Scholar
  18. Emsley, J., Arif, M., Bates, P. & Hursthouse, M. (1988). Bis(acetato)bis[4-(N-acetylamino)pyridine]aquacopper(II)-hydrogen fluoride-hydrate (1/2/2): X-ray structure reveals HO·HF hydrogen bonded in the lattice.1493-1497.
    Open DOISearch in Google Scholar
  19. Aakeroy, C. B., Hussain, I., Forbes, S. & Desper, J. (2007). Exploring the hydrogen-bond preference of N-H moieties in co-crystals assembled via O-H(acid) N(py) intermolecular interactions.9, 46-55.
    Open DOISearch in Google Scholar
  20. Sheldrick, G. M. 1995, SHELXTL, Release 5.03 for Siemens R3 crystallographic research system. Siemens Analytical X-Ray Instruments, Inc., Madison, USA.
    Search in Google Scholar
  21. Sheldrick, G. M. 1997, SHELXS97 and SHELXL97. University of Göttingen, Germany.
    Search in Google Scholar
  22. Ivanova, B. B., Arnaudov, M. G. & Bontchev, P. R. (2004). Linear-dichroic infrared spectral analysis of Cu(I)-homo-cysteine complex.60(4)A, 855-862.
    Open DOISearch in Google Scholar
  23. Ivanova, B. B.; Tsalev, D. L. & Arnaudov, M. G. (2006). Validation of reducing-difference procedure for the interpretation of non-polarized infrared spectra of-component solid mixtures.69, 822-828.
    Open DOISearch in Google Scholar
  24. Ivanova, B. B., Simeonov, V. D., Arnaudov, M. G. & Tsalev, D. L. (2007). Linear-dichroic infrared spectroscopy — validation and experimental design of the orientation technique as suspension in nematic liquid crystal.67A, 66-75.
    Open DOISearch in Google Scholar
  25. Koleva, B. B., Kolev, T., Simeonov, V., Spassov, T. & Spiteller, M. (2008). Linear polarized IR-spectroscopy of partial oriented solids as a colloid suspension in nematic liquid crystal — new tool for structural elucidation of the chemical compounds., 61, 319-333.
    Open DOISearch in Google Scholar
  26. Frisch, M. J., Trucks, G. W., Schlegel, HB., Scuseria, G. E., Robb, M. A., Cheeseman, J. R., Zakrzewski, V. G., Montgomery, Jr. J. A., Stratmann, R. E., Burant, J. C., Dapprich, S., Millam, J. M., Daniels, A. D., Kudin, K. N., Strain, M. C., Farkas, Ö., Tomasi, J., Barone, V., Cossi, M., Cammi, R., Mennucci, B., Pomelli, C., Adamo, C., Clifford, S., Ochterski, J., Petersson, G. A., Ayala, P. Y., Cui, Q., Morokuma, K., Salvador, P., Dannenberg, J. J., Malick, D. K., Rabuck, A. D., Raghavachari, K., Foresman, J. B., Cioslowski, J., Ortiz, J. V., Baboul, A. G., Stefanov, B. B., Liu, G., Liashenko, A., Piskorz, P., Komáromi, I., Gomperts, R., Martin, R. L., Fox, D. J., Keith, T., Al-Laham, M. A., Peng, C. Y., Nanayakkara, A., Challacombe, M., Gill, P. M. W., Johnson, B., Chen, W., Wong, M. W., Andres, J. L., Gonzalez, C., Head-Gordon, M., Replogle, E. S. & Pople, J. A. Gaussian 98, Gaussian, Inc., Pittsburgh, PA, 1998.
    Search in Google Scholar
  27. Zhurko, G. A. & Zhurko, D. A., ChemCraft:, Lite version build 08 2005.
    Search in Google Scholar
DOI: https://doi.org/10.2478/v10026-009-0033-y | Journal eISSN: 3072-0389 (formerly 1899-4741) | Journal ISSN: 1509-8117
Journal RSS Feed
Language: English
Page range: 35 - 40
Published on: Oct 9, 2009
Published by: West Pomeranian University of Technology, Szczecin
In partnership with: Paradigm Publishing Services
Publication frequency: Volume open
Keywords:
4-Acetaminopyridine,
protonated form,
crystal structure,
solid-state linear polarized IRspectroscopy,
UV-spectroscopy,
quantum chemical calculations,
1H- and 13C NMR,
ESI MS,
TGA and DSC
Related subjects:
Industrial chemistry,
Biotechnology,
Chemical engineering,
Process engineering

© 2009 Bojidarka Koleva, Rositsa Nikolova, Atanas Tchapkanov, Tsonko Kolev, Heike Mayer-Figge, Michael Spiteller, William Sheldrick, published by West Pomeranian University of Technology, Szczecin
This work is licensed under the Creative Commons License.

Volume 11 (2009): Issue 3 (September 2009)
Previous article
Next article