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Combustion synthesis process for the rapid preparation of high-purity SrO powders Cover

Combustion synthesis process for the rapid preparation of high-purity SrO powders

Open Access
|Dec 2014

Abstract

A rapid, safe and simple technique for the production of high purity strontium oxide powders via a chemical combustion process is reported. The combustion reactions were performed to optimize the fuel to oxidizer ratios in the reaction mixtures required to obtain pure SrO powders by varying the molar ratio of chemical precursors and the temperature. The synthesized powders were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectrometry, infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and N2-physisorption measurements. The results indicate that crystalline SrO was obtained using a 1:1 strontium nitrate: urea molar ratio at 1000 °C after 5 minutes. In addition, high-purity, homogeneous and crystalline SrO powders were easily produced in a short time via a chemical combustion process.

DOI: https://doi.org/10.2478/s13536-014-0250-9 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 682 - 687
Published on: Dec 19, 2014
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2014 Francisco Granados-Correa, Juan Bonifacio-Martínez, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.