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Synthesis of V2O3/C composites with different morphologies by a facile route and phase transition properties of the compounds Cover

Synthesis of V2O3/C composites with different morphologies by a facile route and phase transition properties of the compounds

Open Access
|Jul 2014

Abstract

V2O3 and amorphous carbon composites (V2O3/C composites) with different morphologies (e.g. nanospheres, nanorods and nanosheets) were, for the first time, successfully synthesized by a facile hydrothermal route and subsequent calcination. The as-obtained samples were characterized by X-ray powder diffraction (XRD), energy dispersive spectrometery (EDS), elemental analysis (EA), Fourier transform infrared spectroscopy (FT-IR), Raman spectroscopy, scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The morphology of V2O3/C composites could be easily controlled by varying the reaction time, and, as a result, V2O3/C composites with nanospheres, nanorods and nanosheets were selectively synthesized. Furthermore, the phase transition property of V2O3/C composites was measured by differential scanning calorimetry (DSC), suggesting that V2O3/C composites exhibit the phase transition similar to V2O3, which could expand the potential applications of materials related to V2O3 in the future.

DOI: https://doi.org/10.2478/s13536-013-0177-6 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 236 - 242
Published on: Jul 22, 2014
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2014 Yifu Zhang, Nannan Wang, Yuting Huang, Chi Huang, Xiao Mei, Changgong Meng, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.