Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Mohammad Fard; Sara Tabaroki

doi:10.2478/s13536-013-0151-3

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Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Materials Science-Poland

Volume 32 (2014): Issue 1 (January 2014)

By: Mohammad Fard and Sara Tabaroki

Open Access

|Mar 2014

Abstract

A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis, elemental analysis and IR spectroscopy. The single crystal X-Ray analysis shows that this polymer is 2-D along a axis. Flower-like nanostructure thallium (III) oxide, Tl2O3 has been prepared by direct thermal decomposition of thallium (I) coordination polymer. The nanostructure was characterized by scanning electron microscopy (SEM), X-Ray powder diffraction (XRD) and IR spectroscopy. The thermal stability of the Tl2O3 nanostructure was studied by thermal gravimetric analysis and differential thermal analysis (TGA /DTA) too.

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Articles in this issue

DOI: https://doi.org/10.2478/s13536-013-0151-3 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331

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Language: English

Page range: 23 - 27

Published on: Mar 26, 2014

Published by: Wroclaw University of Science and Technology

In partnership with: Paradigm Publishing Services

Publication frequency: 4 issues per year

Keywords:

thallium (I),

coordination polymer,

nanostructure,

thallium (III) oxide

Related subjects:

Materials sciences,

Materials sciences, other,

Nanomaterials,

Functional and smart materials,

Materials characterization and properties

© 2014 Mohammad Fard, Sara Tabaroki, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Volume 32 (2014): Issue 1 (January 2014)