Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Fard, Mohammad; Tabaroki, Sara

doi:10.2478/s13536-013-0151-3

Abstract

A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis, elemental analysis and IR spectroscopy. The single crystal X-Ray analysis shows that this polymer is 2-D along a axis. Flower-like nanostructure thallium (III) oxide, Tl2O3 has been prepared by direct thermal decomposition of thallium (I) coordination polymer. The nanostructure was characterized by scanning electron microscopy (SEM), X-Ray powder diffraction (XRD) and IR spectroscopy. The thermal stability of the Tl2O3 nanostructure was studied by thermal gravimetric analysis and differential thermal analysis (TGA /DTA) too.

References

[1] Stumpf H.O., Ouahab L., Pei Y. Grandjean D., Kahn O., Science, 261 (1993), 447. http://dx.doi.org/10.1126/science.261.5120.44710.1126/science.261.5120.447
Search in Google Scholar
[2] Gardner G.B., Venkataraman D.,. Moore J. S., Lee S., Nature, 374 (1995), 792. http://dx.doi.org/10.1038/374792a010.1038/374792a0
Search in Google Scholar
[3] Bruce D.W., Accounts Chem. Res., 33 (2000), 831. http://dx.doi.org/10.1021/ar990159k10.1021/ar990159k
Search in Google Scholar
[4] Moulton B., Lu J., Hajndl R., Hariharan S., Zaworotko M.J., Angew. Chem. Int. Edit., 41 (2002) 2821. http://dx.doi.org/10.1002/1521-3773(20020802)41:15<;2821::AID-ANIE2821>3.0.CO;2-Y10.1002/1521-3773(20020802)41:15<;2821::AID-ANIE2821>3.0.CO;2-Y
Search in Google Scholar
[5] Cleverty A.M., Ward M.D., Accounts Chem. Res., 31 (1998), 842. http://dx.doi.org/10.1021/ar970315s10.1021/ar970315s
Search in Google Scholar
[6] Rashidi Ranjbar Z., Morsali A., J. Mol. Struct., 936 (2009) 206. http://dx.doi.org/10.1016/j.molstruc.2009.07.04110.1016/j.molstruc.2009.07.041
Search in Google Scholar
[7] Morsali A., Tadjarodi R., Mohammadi R., Mahjoub A.R., Z. Krist.-New Cryst. St., 216 (2001) 379.
Search in Google Scholar
[8] Mahjoub A.R., Morsali A., J. Coord. Chem., 56 (2003), 779. http://dx.doi.org/10.1080/009589703100011060010.1080/0095897031000110600
Search in Google Scholar
[9] Morsali A., Payheghader M., Poorheravi M.R., Jamali F.Z., Z. Anorg. Allg. Chem., 629 (2003), 1627. http://dx.doi.org/10.1002/zaac.20030003910.1002/zaac.200300039
Search in Google Scholar
[10] Morsali A., Mahjoub A. R., Darzi S. J., Soltanian M. J., Z. Anorg. Allg. Chem., 629 (2003), 2596. http://dx.doi.org/10.1002/zaac.20030015410.1002/zaac.200300154
Search in Google Scholar
[11] Morsali A., Kempe R., Helv. Chim. Acta, 88 (2005), 2267. http://dx.doi.org/10.1002/hlca.20059016010.1002/hlca.200590160
Search in Google Scholar
[12] Xiao H.P., Morsali A., Helv. Chim. Acta, 88 (2005), 2543. http://dx.doi.org/10.1002/hlca.20059019210.1002/hlca.200590192
Search in Google Scholar
[13] Morsali A., Mahjoub A.R., Solid State Sci., 7 (2005), 1429. http://dx.doi.org/10.1016/j.solidstatesciences.2005.08.01310.1016/j.solidstatesciences.2005.08.013
Search in Google Scholar
[14] Morsali A., Solid State Sci., 8 (2006), 82. http://dx.doi.org/10.1016/j.solidstatesciences.2005.10.00410.1016/j.solidstatesciences.2005.10.004
Search in Google Scholar
[15] Beckman U., Brooker S., Coordin. Chem. Rev., 245 (2003), 17. http://dx.doi.org/10.1016/S0010-8545(03)00030-410.1016/S0010-8545(03)00030-4
Search in Google Scholar
[16] Klingale M.H., Brooker S., Coordin. Chem. Rev., 241 (2003) 119. http://dx.doi.org/10.1016/S0010-8545(03)00049-310.1016/S0010-8545(03)00049-3
Search in Google Scholar
[17] Haasnoot J.G., Coordin. Chem. Rev., 200 (2000), 131. http://dx.doi.org/10.1016/S0010-8545(00)00266-610.1016/S0010-8545(00)00266-6
Search in Google Scholar
[18] Withersby M.A. et al., Inorg. Chem., 38 (1999), 2259. http://dx.doi.org/10.1021/ic980898h10.1021/ic980898h
Search in Google Scholar
[19] Blake A.J., Champness N.R., Cooke P.A., Nicolson J.E.B., Wilson C., J. Chem. Soc. Dalton, (2000), 3811. 10.1039/b003202f
Search in Google Scholar
[20] Withersby M.A., Blake A.J., Champness N.R., Hubberstey P., Li W.S., Schroder M., Angew. Chem. Int. Edit., 36 (1997), 2327. http://dx.doi.org/10.1002/anie.19972327110.1002/anie.199723271
Search in Google Scholar
[21] Notash B., Safari N., Khavasi H. R., Amani V., Abedi A., J. Organomet. Chem., 693 (2008), 3553. http://dx.doi.org/10.1016/j.jorganchem.2008.08.02710.1016/j.jorganchem.2008.08.027
Search in Google Scholar
[22] Akhbari K., Morsali A., Coordin. Chem. Rev., 254 (2010), 1977. http://dx.doi.org/10.1016/j.ccr.2010.03.00610.1016/j.ccr.2010.03.006
Search in Google Scholar
[23] Sheldrick G. M. (2008), SADABS V2008/1, Bruker-AXS Inc, Madison, Wisconsin, USA.
Search in Google Scholar
[24] Sheldrick G. M., Acta Crystallogr. A, 64 (2008) 112. http://dx.doi.org/10.1107/S010876730704393010.1107/S0108767307043930
Search in Google Scholar
[25] Mercury 1.4.1, Copyright Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK, 2001.
Search in Google Scholar
[26] Demko Z.P., Sharpless K. B., J. Org. Chem., 66 (2001), 7945. http://dx.doi.org/10.1021/jo010635w10.1021/jo010635w
Search in Google Scholar
[27] Hazell A., Mcginley J., Toftlund H., Inorg. Chim. Acta., 323 (2001), 113. http://dx.doi.org/10.1016/S0020-1693(01)00609-010.1016/S0020-1693(01)00609-0
Search in Google Scholar
[28] Yang J., Lin C., Wang Zh., Lin J., Inorg. Chem., 45 (2006), 8973. http://dx.doi.org/10.1021/ic060934+10.1021/ic060934
Search in Google Scholar

Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

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