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Preparation and enhanced oil recovery mechanism of dual-shell amphiphobic fluorinated nano-polymer core–shell materials Cover

Preparation and enhanced oil recovery mechanism of dual-shell amphiphobic fluorinated nano-polymer core–shell materials

Open Access
|Apr 2026

Figures & Tables

Figure 1

Synthesis procedure of dual-shell nanomaterials.

Figure 2

Chemical reaction equations for Step 1.

Figure 3

Chemical reaction equations for Step 2.

Figure 4

Chemical reaction equations for shell layer preparation.

Figure 5

Schematic diagram of experimental apparatus for displacement. performance evaluation.

Figure 6

FTIR spectroscopy spectrum.

Figure 7

XPS characterization of dual-shell amphiphobic fluorinated. nanocomposites. (a) Si 2p spectra; (b) C 1s spectra, (c) N 1s spectra, (d) F 1s spectra, (e) O 1s spectra, and (f) surface elemental composition (atomic percentage).

Figure 8

TGA results: (a) TG and (b) DTG.

Figure 9

Contact angle measurements of core samples treated with different materials: (a) Contact angle with water and (b) contact angle with n-hexadecane. Error bars represent standard deviation (n = 8).

Figure 10

Stability test results of different materials. (a) Thermal stability–contact angle with water, (b) thermal stability–contact angle with n-hexadecane, (c) salt resistance–contact angle with water, (d) salt resistance–Ccntact angle with n-hexadecane, (e) durability–contact angle with water, and (f) durability–contact angle with n-hexadecane.

Figure 11

Analysis of stability mechanism.

Figure 12

Evaluation of displacement performance for different materials: (a) Graph of the relationship between displacement volume and pressure and (b) relationship between displacement time and oil recovery efficiency.

Figure 13

Schematic diagram of enhanced oil recovery mechanisms.

Surface elemental composition determined by XPS (atomic %)

MaterialSiOCNF
Pristine SiO2 28.366.84.9
APTES-MAnh22.156.718.23.0
AFPCSMs12.832.137.62.315.2

Surface free energy of rocks with different materials

Material0.01 wt%0.05 wt%0.10 wt%
APTES-MAnh59.72 mN/m51.46 mN/m45.78 mN/m
C-PFOTS37.18 mN/m12.79 mN/m6.20 mN/m
AFPCSMs33.10 mN/m6.18 mN/m1.44 mN/m
Language: English
Page range: 1 - 16
Submitted on: Sep 21, 2025
Accepted on: Jan 2, 2026
Published on: Apr 27, 2026
In partnership with: Paradigm Publishing Services
Publication frequency: Volume open

© 2026 Guojie Sui, Hai Lin, Huan Liu, Tingsong Xiong, Shiduo Liu, Shijun Chen, published by West Pomeranian University of Technology, Szczecin
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.