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Investigation of the mechanical, corrosion, and tribological characteristics of AZ61 Mg with boron carbide nano particles via the stir casting route Cover

Investigation of the mechanical, corrosion, and tribological characteristics of AZ61 Mg with boron carbide nano particles via the stir casting route

Open Access
|Sep 2023

Figures & Tables

Fig. 1.

Fabrication of AZ61/ B4C nanocomposites

Fig. 2.

SEM micrographs of nanocomposites of AZ61/B4C: (a) AZ61 alloy, (b) AZ61/2.5wt%B4C, (c) AZ61/5wt%B4C, (d) AZ61/7.5wt%B4C, (e) AZ61/10wt%B4C

Fig. 3.

EDS analysis of nanocomposites of AZ61/B4C: (a) AZ61 alloy, (b) AZ61/2.5wt%B4C, (c) AZ61/5wt%B4C, (d) AZ61/7.5wt%B4C, (e) AZ61/10wt%B4C

Fig. 4.

AZ61/B4C nanocomposites and the hardness of their relationship

Fig. 5.

(a) AZ61/B4C nanocomposites and the compressive strength of their relationship (b) stressstrain curve of AZ61/B4C nanocomposites

Fig. 6.

AZ61/B4C nanocomposites and the impact strength of their relationship

Fig. 7.

AZ61/ B4C nanocomposites and the flexural strength of their relationship

Fig. 9.

Contour plot: wt% B4C vs. load

Fig. 10.

Contour plot: wt% B4C vs. sliding distance

Fig. 11.

Contour plot: wt% B4C vs. sliding velocity

Fig. 12.

Contour plot: wt% B4C vs. load

Fig. 13.

Contour plot wt% B4C vs. sliding distance

Fig. 14.

Contour plot wt% B4C vs. sliding velocity

Fig. 8.

AZ61/B4C nanocomposites and the corrosion behavior of their relationship

Fig. 15.

Grey relational grade

Fig. 16.

Main effect plot for wear rate

Fig. 17.

Main effect plot for coefficient

Fig. 18.

Normal probability plot

The density of AZ61/B4C nanocomposites

CompositesExperimental densityg/cm3Theoretical densityg/cm3Porosity%
A (AZ61-Mg alloy)1.7851.7901.38
B (AZ61 with 2.5wt% B4C)1.8011.8241.24
C (AZ61 with 5wt% B4C)1.8141.8311.18
D (AZ61 with 7.5wt% B4C)1.8261.8401.07
E (AZ61 with 10wt% B4C)1.8301.8481.04

Corrosion properties of the AZ61/B4C nanocomposites

CompositesIcorr(mA/cm2)Ecorr(mV)Corrosion rate(mils/yr)
A0.0039751−753.15355.37
B0.0032398−856.25338.70
C0.0030175−869.60320.96
D0.0021956−916.36220.47
E0.0024096−909.77240.36

Grey relational grade response table

LevelWt%L (N)SV (m/s)SD (m)
14.4695.9545.0174.925
25.0036.0245.4175.363
33.6594.9745.4785.913
47.9214.0995.1394.851
Delta4.2621.9250.461.062
Rank1243

Calculated S/N ratio as well as the normalized S/N ratio

S/N ratio for wearS/N ratio for COFNormalization for wearNormalization for COF
41.51446.33910.8740.000
42.38375.58030.7860.177
41.20966.21380.9050.029
40.26465.02071.0000.307
46.19614.48050.4010.433
42.49884.35050.7750.463
43.45263.28620.6780.711
42.05854.62720.8190.399
50.17282.22520.0000.959
46.93573.16030.3270.741
45.84862.34950.4360.930
43.34982.04750.6891.000
50.17284.65690.0000.392
48.17876.14310.2010.046
46.37525.66320.3830.157
46.00324.94370.4210.325

ANOVA for Grey relational grade

SourceDFAdj SSAdj MSF ValueP ValueContribution %
Wt%30.1481760.04939216.670.02267.19
L (N)30.0457230.0152415.140.10620.73
SV (m/s)30.0014330.0004780.160.9160.65
SD (m)30.0163020.0054341.830.3157.39
Error30.0088890.002963
Total150.220523

Tensile characteristics of AZ61/B4C nanocomposites

CompositesUltimate tensile strength (MPa)Yield strength (MPa)Elongation (%)
A15810110.4
B1661148.6
C1781266.8
D1941385.6
E1821296.0

Calculated deviation sequences for GRC and GRG

Deviation sequence for wearDeviation sequence for COFGRC for wearGRC for COFGRGRank
0.1261.0000.7990.3330.5669
0.2140.8230.7000.3780.53911
0.0950.9710.8400.3400.5907
0.0000.6931.0000.4190.7102
0.5990.5670.4550.4690.46212
0.2250.5370.6890.4820.5868
0.3220.2890.6080.6340.6215
0.1810.6010.7340.4540.5946
1.0000.0410.3330.9240.6284
0.6730.2590.4260.6580.54210
0.5640.0700.4700.8770.6733
0.3110.0000.6161.0000.8081
1.0000.6080.3330.4510.39215
0.7990.9540.3850.3440.36416
0.6170.8430.4480.3720.41014
0.5790.6750.4630.4260.44413

Experimental results

Exp. No.Wt% B4CL (N)SV (m/s)SD (m)WR (mm3/m)COF
10414000.00840.482
20828000.00760.526
3012312000.00870.489
4016416000.00970.561
52.54212000.00490.597
62.58116000.00750.606
72.51244000.006720.685
82.51638000.007890.587
954316000.00310.774
1058412000.00450.695
1151218000.00510.763
1251624000.00680.79
137.5448000.00310.585
147.5834000.00390.493
157.512216000.00480.521
167.516112000.005010.566
DOI: https://doi.org/10.2478/msp-2023-0019 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 227 - 243
Submitted on: Jan 28, 2023
|
Accepted on: Jul 17, 2023
|
Published on: Sep 19, 2023
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2023 S. Sakthi, S. Mahendran, M. Meignanamoorthy, V. Mohanavel, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.