Synthesis, electrical and magnetic properties of polymer coated magnetic nanoparticles for application in MEMS/NEMS

Javid, Muhammad Arshad; Sajjad, Muhammad; Ahmad, Saeed; Khan, Muhammad Azhar Shahid; Nadeem, Khalid; Amin, Niama; Mehmood, Zahid

doi:10.2478/msp-2020-0080

Abstract

In this research work, polymer coated magnetic nanoparticles were prepared by co-precipitation method. The samples were characterized by XRD, SEM, EDS, VSM and two probe DC conductivity measurements. XRD pattern indicated the existence of a sole cubic phase of Fe₃O₄ with Miller indices (2 2 0), (3 1 1), (5 1 1), (4 4 0). An average size of magnetic nanoparticles was about 22.9 nm and it was reduced to 21.3 nm and 19.4 nm after 1 wt. %. and 2 wt. % coating of PEG-6000, respectively. The morphology and size of the samples were investigated by scanning electron microscope (SEM). EDX spectra confirmed the coating of PEG on magnetic nanoparticles. Magnetic properties were examined by vibrating sample magnetometer (VSM). Saturation magnetization (M_s) decreased as the concentration of PEG increased in the magnetic material. Electrical properties of uncoated and polymer coated Fe₃O₄ nanoparticles were studied by two-probe conductivity meter. This study concluded that the thermal flow of charge in polymer coated magnetic nanoparticles can be evaluated at micro and nano level.

References

[1] Oliveira D., Barud S., Salvi D., Perotti G., Riberio S., Indian Crop. Prod., 69, (2015), 415.10.1016/j.indcrop.2015.02.015
Search in Google Scholar Back to article
[2] Xu H., Cheng L., Wang C., Ma X., Li Y., Liu Z., Biomaterials, 32: (2011), 9364.10.1016/j.biomaterials.2011.08.05321880364
Search in Google Scholar Back to article
[3] Chai C.C., Lee Z.H., Toh P.Y., Chieh C.J, Ahmad A.L., Lim J.K., Chem. Eng. J., 281, (2015), 523.10.1016/j.cej.2015.06.108
Search in Google Scholar Back to article
[4] Hauser A.K., Wydra R.J., Stocke A., Anderson W., Hilt Z., J. Cont. Rel., 219, (2015), 76.10.1016/j.jconrel.2015.09.039466906326407670
Search in Google Scholar Back to article
[5] Leng J., Li J., Ren J., Deng L., Lin C., Mater. Lett., 152, (2015), 185.10.1016/j.matlet.2015.03.120
Search in Google Scholar Back to article
[6] Heid A., Bahrololoom M., Vashaee D., Tayebi I., Ceramic. International., 41, (2015), 3094.10.1016/j.ceramint.2014.10.153
Search in Google Scholar Back to article
[7] Omidi H.M., Mahboobeh A., Farideh P., Materials Science-Poland 35, (2017), 105-110.10.1515/msp-2017-0011
Search in Google Scholar Back to article
[8] Sun X., Keating A., Parish G., Micropor. Mesopor. Mat., 218, (2015), 88.10.1016/j.micromeso.2015.07.010
Search in Google Scholar Back to article
[9] Thangawng A.L., Rodney S.R., Melody A.S., Biomedical Microdevices 9, (2007), 587-595.10.1007/s10544-007-9070-617516172
Search in Google Scholar Back to article
[10] Javid MA., Sadaqat N., Rafique M., Materials Today: Proceedings. (2020).
Search in Google Scholar Back to article
[11] Javid Ma., U.Zafar, H.Fayyaz, M.Imran., Int. J. Mod. Phys. B, 32 (14), (2018), 13.
Search in Google Scholar Back to article
[12] Javid MA., Fayyaz H., Imran M., Mater. Sci.- Poland, 34, (2016), 741.10.1515/msp-2016-0109
Search in Google Scholar Back to article
[13] Azeem N., Ma. Javid, Tahir I., J. Semicond, 38. (2017), 7.
Search in Google Scholar Back to article
[14] Sabater AB., Jeff R., J. Micromech. Microeng., 24, (2014), 065005.10.1088/0960-1317/24/6/065005
Search in Google Scholar Back to article
[15] Narbutovskih M., Field L., Clifford G., Beck P., Sensor. Actuat. A-Phys., 70, (1998), 128.10.1016/S0924-4247(98)00123-X
Search in Google Scholar Back to article
[16] Kim S., Roy S., Adv. Chronic. Kidney D, 20, (2013), 516.10.1053/j.ackd.2013.08.006386602024206604
Search in Google Scholar Back to article
[17] Attallah A., Girgis E., J. Magn. Magn. Mater., 399, (2016), 58.10.1016/j.jmmm.2015.09.059
Search in Google Scholar Back to article
[18] Manrique J., Machuca F., Marriga F., J. Magn. Magn. Mater., 401, (2016), 81.10.1016/j.jmmm.2015.10.018
Search in Google Scholar Back to article
[19] Li X., Liu G., Yan W., Chu P.K., Wu S., Yi C., Xu Z., J. Magn. Magn. Mater., 324, (2012), 1410.10.1016/j.jmmm.2011.11.056
Search in Google Scholar Back to article
[20] Cantalapiedra A., Gismera M.J., Procopio JR., Sevilla M.T., Talanta, 139, (2015), 111.10.1016/j.talanta.2015.02.04925882415
Search in Google Scholar Back to article
[21] Cornell R.M., Schwertmann U., The iron oxides. VCH Press, Weinheim, Germany, (1996).
Search in Google Scholar Back to article
[22] Arshad J., Saddique A., Zahid M., Mater. Sci- Poland, 25 (2019), 359.10.5755/j01.ms.25.4.21149
Search in Google Scholar Back to article
[23] Javid M.A., Materials Today: Proceedings (2020).
Search in Google Scholar Back to article
[24] Harsha N., Swathi K., Neeroli K.R., Satyajit S., RSC Adv., 38, (2015), 30354.10.1039/C5RA03722K
Search in Google Scholar Back to article
[25] Takenaka K., Ozawa A., Shibayama T., Urano C., Appl. Phys. Letters; 9 (2011), 022103.10.1063/1.3541449
Search in Google Scholar Back to article
[26] Katikaneani P., Ajay K V., Narender RT., Ramu B., Srivani K., J. Nanosci., (2016).
Search in Google Scholar Back to article
[27] Shanmuga SI., Mayank S., Shampa S., Transl. Biomed., 6,3: (2015).
Search in Google Scholar Back to article
[28] Franco A., Thiago AL., Emília LI., Eloisa N., Appl. Phys. A, 94 (1) (2009), 131.
Search in Google Scholar Back to article
[29] Markhulia J., Mikelashvili V., Kekutia L., J. Pharm. Appl. Chem., 2, (2016), 33.10.18576/jpac/020201
Search in Google Scholar Back to article
[30] Khalkhali M., Rostamizadeh K., Sadighian S., J. Pharm. Sci., 23 (2015), 45.10.1186/s40199-015-0124-7
Search in Google Scholar Back to article
[31] Mahdavi M., Ahmad B., Haron J., Rahman A., J., Molecules, 18 (2013), 7533.10.3390/molecules18077533
Search in Google Scholar Back to article
[32] Anbarasu M., Anandan E., Chinnasamy V., Gopinath K., Spectrochim. Acta A, 135 (2015), 536.10.1016/j.saa.2014.07.059
Search in Google Scholar Back to article
[33] Yunas J., Polymers, 5 (2020), 1184.10.3390/polym12051184
Search in Google Scholar Back to article
[34] Vella L., Emerson D., ASEG Extended Abstracts, 1 (2012), 1.10.1071/ASEG2012ab232
Search in Google Scholar Back to article
[35] Schwertmann U., Rochelle MC., Iron oxides in the laboratory: preparation and characterization. John Wiley & Sons, 2008.
Search in Google Scholar Back to article
[36] Eslamian M., Morteza M., Ziad S., Fluid Dynamics and Material Processing, 2012.
Search in Google Scholar Back to article
[37] Weidenfeller E., Höfer M., Frank S., Composites Part A: Appl. Sci. Manuf, 33, (2002), 1041.10.1016/S1359-835X(02)00085-4
Search in Google Scholar Back to article
[38] Cimalla V., Joerg P., Oliver A., J. Physics D: Appl. Phys, 40, 20 (2007), 6386.10.1088/0022-3727/40/20/S19
Search in Google Scholar Back to article

Synthesis, electrical and magnetic properties of polymer coated magnetic nanoparticles for application in MEMS/NEMS

Abstract

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