Have a personal or library account? Click to login
In-house validation method for quantification of amoxicillin in medicated feedingstuffs with the use of HPLC-DAD technique Cover

In-house validation method for quantification of amoxicillin in medicated feedingstuffs with the use of HPLC-DAD technique

Open Access
|Jun 2020

References

  1. Ang C.Y.W., Luo W.H., Hansen E.B., Freeman J.P., Thompson H.C. Jr.: Determination of amoxicillin in catfish and salmon tissues by liquid chromatography with precolumn formaldehyde derivatization. J AOAC Intern 1996, 79, 389–396.
  2. Association of American Feed Control Officials (AAFCO): Reference method AOAC 967.41(Code AAFCO 074.00) in Feed Check Samples, 2006, AAFCO, Champaign, IL, USA.
  3. Becker M., Zittlaub E., Petza M.: Residue analysis of 15 penicillins and cephalosporins in bovine muscle, kidney, and milk by liquid chromatography–tandem mass spectrometry. Anal Chim Acta 2004, 520, 19–32.
  4. Benito-Pena E., Urraca J.L., Moreno-Bondi M.C.: Quantitative determination of penicillin V and amoxicillin in feed samples by pressuurised liquid extraction and liquid chromatography with ultraviolet detection. J Pharm Biomed Anal 2009, 49, 289–294.
  5. Bo W., Maoda P., Xing X., Min Z., Kaizhou X., Yangyang Z., Xia Z., Ya’juan W., Ran W., Haiqing W., Genxi Z., Guojun D., Jinyu W.: Quantitative analysis of amoxicillin, amoxicillin major metabolites, and ampicillin in chicken tissues via ultra-performance liquid chromatography-electrospray ionization tandem mass spectrometry. Food Anal Methods 2017, 10, 3292– 3305.
  6. Bogialli S., Capitolino V., Curini R., Di Corcia A., Nazzari M., Sergi M.: Simple and rapid liquid chromatography−tandem mass spectrometry confirmatory assay for determining amoxicillin and ampicillin in bovine tissues and milk. J Agri Food Chem 2004, 52, 3286–3291.
  7. Chuangji L., Hai W., Yanbin J., Zhenxia D.: Rapid and simultaneous determination of amoxicillin, penicillin G, and their major metabolites in bovine milk by ultra-high-performance liquid chromatography–tandem mass spectrometry. J Chromatogr B 2011, 879, 533–540.
  8. Cutting J.H., Hurlbut J.A., Sofos J.N.: Quantitation of penicillin G in medicated premix feeds by micellar electrokinetic capillary chromatography. J AOAC Inter 1997, 80, 951–955.
  9. De Baere S., De Backer P.: Quantitative determination of amoxicillin in animal feed using liquid chromatography with tandem mass spectrometric detection. Anal Chim Acta 2007, 586, 319–325.
  10. European Medicines Agency: 8th ESVAC Report 2018. Sales of veterinary antimicrobial agents in 30 European countries in 2016 Trends from 2010 to 2016. London, 2018.
  11. Fernandez-Torres R., Olias Consentino M., Bello M.A., Callejon M.: Simultaneous determination of 11 antibiotics and their main metabolites from four different groups by reversed-phase high-performance liquid chromatography–diode array–fluorescence (HPLC–DAD–FLD) in human urine samples. Talanta 2010, 81, 871–880.
  12. Gamba V., Dusi G.: Liquid chromatography with fluorescence detection of amoxicillin and ampicillin in feeds using pre-column derivatization. Anal Chim Acta 2003, 483, 69–72.
  13. Heller D.N., Ngoh M.A.: Electrospray ionization and tandem ion trap mass spectrometry for the confirmation of seven β-lactam antibiotics in bovine milk. Rapid Communicat Mass Spectrometry 1998, 12, 2031–2040.
  14. Hui L., Xi X., Yanan X., Shusheng T., Xilong X., Jiancheng L., Jianzhong S.: Simultaneous determination of amoxicillin and prednisolone in bovine milk using ultra-high performance liquid chromatography tandem mass spectrometry. J Chromatogr B 2012, 900, 59–63.
  15. Krasucka D., Kowalski C.J., Osypiuk M.: Determination of amoxicillin in pig plasma by liquid chromatography with fluorescence detection. Bull Vet Inst Pulawy 2011, 55, 771–775.
  16. LaCourse W.R., Dasenbrock C.O.: Pulsed electrochemical detection of sulfur-containing antibiotics following high performance liquid chromatography. J Pharm Biomed Anal 1999, 19, 239–252.
  17. Lal J., Paliwal J.K., Grover P.K., Gupta R.C.: Determination of ampicillin in serum by high-performance liquid chromatography with precolumn derivatization. J Chrom B 1994, 655, 142–146.
  18. Li Y.M., Van Schepdael A., Zhu Y., Roets E., Hoogmartens J.: Development and validation of amoxicillin determination by micellar electrokinetic capillary chromatography. J Chrom A 1998, 812, 227–236.
  19. Lirui S., Long fei J., Xing X., Kaizhou X., Jianfeng W., Jianyu L., Lulu C., Genxi Z., Guojun D., Jinyu W.: Quantitative analysis of amoxicillin, its major metabolites and ampicillin in eggs by liquid chromatography combined with electrospray ionization tandem mass spectrometry. Food Chem 2016, 192, 313–318.
  20. Lott A.F., Smither R., Vaughan D.R.: Antibiotic identification by high-voltage electrophoresis bioautography. J AOAC Inter 1985, 68, 1018–1020.
  21. Luo W., Hansen E.B. Jr., Ang C.Y.W., Deck J., Freeman J.P., Thompson H.C. Jr.: Simultaneous determination of amoxicillin and ampicillin in bovine milk by HPLC with fluorescence detection. J Agri Food Chem 1997, 45, 1264–1268.
  22. Luo W.H., Ang C.Y.W., Thompson H.C. Jr.: Rapid method for the determination of ampicillin residues in animal muscle tissues by high-performance liquid chromatography with fluorescence detection. J Chrom B 1997, 694, 401–407.
  23. Makeswaran S., Patterson I., Points J.: An analytical method to determine conjugated residues of ceftiofur in milk using liquid chromatography with tandem mass spectrometry. Anal Chim Acta 2005, 529, 151–157.
  24. Mitchell J.M., Griffiths M.W., McEven S.A., McNab W.B., Yee A.J.: Antimicrobial drug residues in milk and meat: causes, concerns, prevalence, regulations, tests, and test performance. J Food Protect 1998, 61, 742–756.
  25. Pajchel G., Pawlowski K., Tyski S.: CE versus LC for simultaneous determination of amoxicillin/clavulanic acid and ampicillin/sulbactam in pharmaceutical formulations for injections. J Pharm Biomed Anal 2002, 29, 75–81.
  26. Patyra E., Kwiatek K.: Development and validation of multi-residue analysis for tetracycline antibiotics in feed by high performance liquid chromatography coupled to mass spectrometry. Food Add Contamin Part A 2017, 34, 1553–1561.
  27. Regulation (EU) 2019/4 of the European Parliament and of the Council of 11 December 2018 on the manufacture, placing on the market and use of medicated feed, amending Regulation (EC) No 183/2005 of the European Parliament and of the Council and repealing Council Directive 90/167/EEC (Text with EEA relevance). OJ L 4, 62, 1–23.
  28. Reyns T., Cherlet M., Baere S.D., Backer P.D., Croubels S.: Tissue depletion of amoxicillin and its major metabolites in pigs: influence of the administration route and the simultaneous dosage of clavulanic acid. J Chrom B 2008, 861, 108–116.
  29. Riediker S., Stadler R.H.: Simultaneous determination of five β-lactam antibiotics in bovine milk using liquid chromatography coupled with electrospray ionization tandem mass spectrometry. Anal Chem 2001, 73, 1614–1621.
  30. Stolker A.A.M., Rutgers P., Oosterink E., Lasaroms J.J.P., Peters J.R.J.B., van Rhijn A., Nielen M.W.F.: Comprehensive screening and quantification of veterinary drugs in milk using UPLC–ToF-MS. Anal Bioanal Chem 2008, 391, 2309–2322.
  31. Tollefson L., Miller M.A.: Antibiotic use in food animals: controlling the human health impact. J AOAC Inter 2000, 83, 245–254.
  32. Xie K., Jia L., Xu D., Guo H., Xie X., Huang Y., Chen X., Bao W., Dai Gu., Wang J.: Simultaneous determination of amoxicillin and ampicillin in eggs by reversed-phase high-performance liquid chromatography with fluorescence detection using pre-column derivatization. J Chrom Sci 2012, 50, 620–624.
  33. Yuan L., Kui Z., Jian Fen W., Xiaoyong H., Guanlin W., Congying L., Jie C., Shuangyang D.: Simultaneous detection and comparative pharmacokinetics of amoxicillin, clavulanic acid, and prednisolone in cows’ milk by UPLC–MS/MS. J Chromatogr B 2016, 1008, 74–80.
Language: English
Page range: 433 - 438
Submitted on: Dec 9, 2019
Accepted on: Jun 10, 2020
Published on: Jun 20, 2020
Published by: National Veterinary Research Institute in Pulawy
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2020 Ewelina Patyra, Krzysztof Kwiatek, published by National Veterinary Research Institute in Pulawy
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.