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Comparison of Select Analytes from Different Laboratories in Tobacco and Smoke for Commercial Cigars Across a Range of Designs Cover

Comparison of Select Analytes from Different Laboratories in Tobacco and Smoke for Commercial Cigars Across a Range of Designs

Open Access
|Jan 2025

References

  1. Abrokwah, R.Y. and R. Tayyarah: Advancements and Challenges of Cigar Science, Testing and Regulation: A Review; Contrib. Tob. Nicotine Res. 32 (2022) 73–89. DOI: 10.2478/cttr-2022-0008
  2. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Methods; TTPA – Tobacco and Tobacco Products Analysis and SA – Smoke Analysis Subgroups; CORESTA, Paris, France. Available at: https://www.coresta.org/ (accessed September 2024)
  3. University of Kentucky (UK), Center for Tobacco Reference Products (CTRP): Cigar Reference Products; CTRP, Lexington, KY, USA. Available at: https://ctrp.uky.edu/products/gallery/Cigars (accessed September, 2024)
  4. U.S. Food and Drug Administration (FDA): Family Smoking Prevention and Tobacco Control Act – An Overview (“Tobacco Control Act”) (21 USC § 387) FDA, Silver Springs, MD, USA, 2009. Available at: https://www.fda.gov/tobacco-products/rules-regulations-and-guidance/family-smoking-prevention-and-tobacco-control-act-overview (accessed September 2024)
  5. U.S. Food and Drug Administration (FDA): Revised Extension of Certain Tobacco Product Compliance Deadlines Related to the Final Deeming Rule; August 2017. Available at: https://www.regulations.gov/docket/FDA-2017-D-2834 (accessed September, 2024)
  6. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): Cigar Smoke Analysis - 15th Collaborative Study 2021, CSM Technical Report, CORESTA, Paris, France. Available at: https://www.coresta.org/cigar-smoke-analysis-15th-collaborative-study-35615.html (accessed September 2024)
  7. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): 2019 Collaborative Study for B[a]P and TSNA Compounds in Mainstream Cigar Smoke; SA Report, June 2022, CORESTA, Paris, France. Available at: https://www.coresta.org/2019-collaborative-study-bap-and-tsna-compounds-mainstream-cigar-smoke-36360.html (accessed September 2024)
  8. U.S. Food and Drug Administration (FDA): Reporting Harmful and Potentially Harmful Constituents in Tobacco Products and Tobacco Smoke Under Section 904(a)(3) of the Federal Food, Drug, and Cosmetic Act Draft Guidance for Industry April 2012, FDA, Rockville, MD, USA. Available at: https://www.fda.gov/regulatory-information/search-fda-guidance-documents/reporting-harmful-and-potentially-harmful-constituents-tobacco-products-and-tobacco-smoke-under (accessed September 2024)
  9. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 46 - Atmosphere for Conditioning and Testing Cigars of All Sizes and Shapes, June 2018, second edition, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_46-June2018.pdf (accessed September 2024)
  10. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 64 – Routine Analytical Cigar-Smoking Machine – Specifications, Definitions and Standard Conditions; May 2018 – second edition, CORESTA, Paris, France. Available at: https://www.coresta.org/routine-analytical-cigar-smoking-machine-specifications-definitions-and-standard-conditions-29187 (accessed September 2024)
  11. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 65 – Determination of Total and Nicotine-Free Dry Particulate Matter using a Routine Analytical Cigar-Smoking Machine – Determination of Total Particulate Matter and Preparation for Water and Nicotine Measurements; August 2019 – fifth edition, CORESTA, Paris, France. Available at: https://www.coresta.org/determination-total-and-nicotine-free-dry-particulate-matter-using-routine-analytical-cigar-smoking (accessed September 2024)
  12. International Organization for Standardization (ISO): ISO 2971:2013 Cigarettes and Filter Rods – Determination of Nominal Diameter – Method Using a Non-Contact Optical Measuring Apparatus; Edition 4, 2013, ISO, Geneva, Switzerland. https://www.iso.org/standard/54738.html. (accessed September 2024)
  13. International Organization for Standardization (ISO): ISO 6565:2015 Tobacco and Tobacco Products – Draw Resistance of Cigarettes and Pressure Drop of Filter Rods – Standard Conditions and Measurement; Edition 5, 2015, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/64265.html (accessed September 2024)
  14. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 62 – Determination of Nicotine in Tobacco and Tobacco Products by Gas Chromatographic Analysis; December 2021, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_62-December2021.pdf (accessed September 2024)
  15. International Organization for Standardization (ISO): ISO 15152:2003 Tobacco – Determination of the Content of Total Alkaloids as Nicotine – Continuous-Flow Analysis Method; Edition 1, 2003, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/26506.html (accessed September 2024)
  16. International Organization for Standardization (ISO): ISO 21045:2018 Cigarettes – Tobacco and Tobacco Products – Determination of Ammonia – Method Using Ion Chromatographic Analysis; Edition 1, 2018, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/69733.html (accessed September 2024)
  17. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 86 – Determination of Select Carbonyls in Tobacco And Tobacco Products by UHPLC-MS/MS; December 2021, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_86-December2021.pdf (accessed September 2024)
  18. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 93 – Determination of Selected Metals in Tobacco Products by ICP-MS; December 2021 - second edition, CORESTA, Paris, France. Available at: https://www.coresta.org/determination-selected-metals-tobacco-products-icp-ms-33784.html (accessed September 2024)
  19. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 82 – Determination of Benzo[a]Pyrene in Tobacco and Tobacco Products by GC-MS; December 2021, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_82-December2021.pdf (accessed September 2024)
  20. International Organization for Standardization (ISO): ISO 21766:2021 Tobacco and Tobacco Products – Determination of Tobacco-Specific Nitrosamines in Tobacco Products – Method Using LC-MS/MS; Edition 2, 2012, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/81666.html. (accessed September 2024)
  21. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 66 – Determination of Nicotine in the Mainstream Smoke of Cigars by Gas Chromatographic Analysis; March 2020, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_66-March2020.pdf (accessed September 2024)
  22. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 67 – Determination of Water in the Mainstream Smoke of Cigars by Gas Chromatographic Analysis; March 2020, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_67-March2020.pdf (accessed September 2024)
  23. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 68 – Determination of Carbon Monoxide in the Mainstream Smoke of Cigars by Non-Dispersive Infrared Analysis; March 2020 – second edition, CORESTA, Paris, France. Available at: https://www.coresta.org/determination-carbon-monoxide-main-stream-smoke-cigars-non-dispersive-infrared-analysis-29191.html (accessed September 2024)
  24. International Organization for Standardization (ISO): ISO 23919:2020 Cigarettes – Determination of Ammonia in Cigarette Mainstream Smoke Using Ion Chromatography; Edition 1, 2020, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/77345.html (accessed September 2024)
  25. International Organization for Standardization (ISO): ISO 21160:2018 Cigarettes – Determination of Selected Carbonyls in the Mainstream Smoke of Cigarettes – Method Using High Performance Liquid Chromatography; Edition 1, 2018, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/69993.html (accessed September 2024)
  26. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 95 – Determination of Aromatic Amines in Mainstream Cigarette Smoke by Gas Chromatography Mass Spectrometry With Negative Chemical Ionisation (GC/MS(NCI)); January 2021, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_95-Jan2021.pdf (accessed September 2024)
  27. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CORESTA Recommended Method No. 58 – Determination of Benzo[a]Pyrene in Mainstream Cigarette Smoke by GC-MS; November 2019, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/CRM_58-Nov2019.pdf (accessed September 2024)
  28. Wagner, K.A., NH. Finkel, J.E. Fossett, and I.G. Gillman: Development of a Quantitative Method for the Analysis of Tobacco-Specific Nitrosamines in Mainstream Cigarette Smoke Using Isotope Dilution Liquid Chromatography/Electrospray Ionization Tandem Mass Spectrometry; Anal. Chem. 77 (2005) 1001–1006. DOI: 10.1021/ac048887v
  29. International Organization for Standardization (ISO): ISO 21330:2018 Cigarettes – Determination of Selected Volatile Organic Compounds in the Mainstream Smoke of Cigarettes – Method Using GC/MS; Edition 1, 2018, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/70555.html (accessed September 2024)
  30. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): Smoke Analysis Sub-Group Technical Report 2021 – Collaborative Study of CORESTA Monitor 9 (CM9) for the Determination of Test Piece Weight, TPM, Water, Nicotine, NFDPM, Carbon Monoxide and Puff Count Obtained Under Mainstream ‘Non-Intense’ and ‘Intense’ Smoking Regimes; March 2022, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/SA-306-CTR_CM9-CollStudy2021_March2022.pdf (accessed September 2024)
  31. National Institute of Health (NIH) NIH RePort: Cigar Reference Products Program – Project Number 5UC2FD006890-02, RePORT, NIH, 2021. Available at: https://reporter.nih.gov/search/La7AngoXP0mgQQY4X39rWA/project-details/10063874 (accessed September 2024)
  32. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA), Tobacco and Tobacco Products Analytes Sub-Group: Technical Report – University of Kentucky Cigar Reference Products 2021 Analysis; September 2021, CORESTA, Paris, France. Available at: https://www.coresta.org/sites/default/files/technical_documents/main/TTPA-282-CTR_UK-Cigar-Reference-Products-2021-Analysis_Sept2021.pdf (accessed September 2024)
  33. Lindegaard, T.: Scientific and Regulatory Challenges for Machine Made Cigars; Presentation 99b from Workshop: Machine Made Cigar Leaf and Product Workshop; 72nd Tobacco Science Research Conference (TSRC), Memphis, TN, USA, 2018, Abstract 99b. Available at: https://www.coresta.org/abstracts/machine-made-cigar-leaf-and-product-workshop-31734.html (accessed September 2024)
  34. Tayyarah, R.: Multiple Point in Time Evaluation of Commercial and Reference Cigarette Products for Abbreviated HPHC Yield for Mainstream Smoke and Filler; CORESTA Congress 2013, Seville, Spain, Presentation ST59. Available at: https://www.coresta.org/sites/default/files/abstracts/2013_ST59_Tayyarah_print.pdf (accessed September 2024)
  35. International Organization for Standardization (ISO): Technical Committees ISO/TC 126 Tobacco and Tobacco Products; ISO, Geneva, Switzerland. Available at: https://www.iso.org/committee/52158.html (accessed September 2024)
  36. International Organization for Standardization (ISO): ISO 3303:2012 Routine Analytical Cigarette Smoking Machine – Definitions and Standard Conditions; Edition 5, 2012, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/60404.html (accessed September 2024)
  37. International Organization for Standardization (ISO): ISO 20778:2018 Cigarettes – Routine Analytical Cigarette Smoking Machine – Definitions and Standard Conditions With an Intense Smoking Regime; Edition 1, 2018, ISO, Geneva, Switzerland. Available at: https://www.iso.org/standard/69065.html (accessed September 2024)
  38. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CSM – Cigar Smoking Methods – 2006; CORESTA, Paris, France. Available at: https://www.coresta.org/groups/cigar-smoking-methods (accessed September 2024).
  39. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): Cigar Smoke Analysis – 16th Collaborative Study – CSM Technical Report; September 2023, CORESTA, Paris, France. Available at: https://www.coresta.org/cigar-smoke-analysis-16th-collaborative-study-37879.html (accessed September 2024)
  40. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): Cigar Smoke Analysis – 13th Collaborative Study – CSM Technical Report; May 2019, CORESTA, Paris, France. Available at: https://www.coresta.org/cigar-smoke-analysis-13th-collaborative-study-32427.html (accessed September 2024)
  41. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): 2017 Collaborative Study of CORESTA Monitor 8 (CM8) for the Determination of Test Piece Weight, TPM, Water, Nicotine, NFDPM, Carbon Monoxide and Puff Count Obtained Under Mainstream ‘ISO’ and ‘Intense’ Smoking Regimes; RAC Technical Report, November 2017, CORESTA, Paris, France. Available at: https://www.coresta.org/2017-collaborative-study-coresta-monitor-8-cm8-determination-test-piece-weight-tpm-water-nicotine (accessed September 2024)
  42. Prepelitskaya, Y., K. Spangler, J.H. Smith., K.C. Avery, J. Wilkinson, M.S. Melvin, and J.H. Miller IV: Are Available Test Methods for the Determination of Ammonia in Mainstream Cigarette Smoke Fit for the Analysis of Cigars?; CORESTA Meeting, Smoke Science/Product Technology, 2017, Kitzbühel, ST 05. https://www.coresta.org/sites/default/files/abstracts/2017_ST05_Prepelitskaya.pdf (accessed September 2024)
  43. Prepelitskaya, Y., J.H. Miller, M. Rusyniak, F.S. Higgins, K.C. Avery, M. Crosswhite, S. Spicer-Glave, and N. Shah: Are Available Test Methods for the Determination of Ammonia in Mainstream Cigarette Smoke Fit for the Analysis of Cigars? - Part 2; 72th Tobacco Science Research Conference (TSRC), 2018, Memphis, Tennessee, USA, Abstr. 094. Available at: https://www.coresta.org/abstracts/are-available-test-methods-determination-ammonia-mainstream-cigarette-smoke-fit-analysis-1 (accessed September 2024)
  44. Tayyarah, R., M.J. Morton, and J.W. Flora: HPHC Testing of Tobacco and Smoke to Examine Cigarette Temporal Variability; Contr. Tob. Nicotine Res. 32 (2022) 112–126. DOI: 10.2478/cttr-2022-0011
  45. Cooperation Centre for Scientific Research Relative to Tobacco (CORESTA): CSM-391-CTR Study of the Long Term Variability of HPHCs in Commercial Cigars; In progress, CORESTA, Paris, France. Available at: https://www.coresta.org/study-groups/active-projects (accessed September 2024)
Language: English
Page range: 234 - 252
Published on: Jan 7, 2025
Published by: Institut für Tabakforschung GmbH
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2025 Rana Tayyarah, Leona R. Sirkisoon, Lee Gentry, published by Institut für Tabakforschung GmbH
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