Have a personal or library account? Click to login
Development of method of isolation and purification of PAHs from exposed semipermeable membrane devices (SPMDs) prior to GC-MS analysis Cover

Development of method of isolation and purification of PAHs from exposed semipermeable membrane devices (SPMDs) prior to GC-MS analysis

Open Access
|Nov 2013

Abstract

Surface water pollution by organic contaminants was investigated using passive sampling by semipermeable membrane devices (SPMDs), based on free transfer of analyte (diffusion) from water into receiving phase of sampler. The work was aimed at isolation method of contaminants from passive samplers extracts and instrumental analysis of polycyclic aromatic hydrocarbons. Gel permeation chromatography after silica gel sample cleanup was used as a method for cleaning the extracts of passive samplers from interfering Triolein, the receiving phase in the samplers. The efficiency of isolation and cleaning was determined for polycyclic aromatic hydrocarbons as a target group of contaminants. Polycyclic aromatic hydrocarbons were determined in the obtained fraction by gas chromatography coupled with mass spectrometry.

DOI: https://doi.org/10.2478/acs-2013-0041 | Journal eISSN: 1339-3065 | Journal ISSN: 1337-978X
Language: English
Page range: 281 - 287
Published on: Nov 23, 2013
Published by: Slovak University of Technology in Bratislava
In partnership with: Paradigm Publishing Services
Publication frequency: 2 issues per year
Related subjects:

© 2013 Veronika Klučárová, Eva Benická, Branislav Vrana, published by Slovak University of Technology in Bratislava
This work is licensed under the Creative Commons License.