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Morphologies of nanostructured bismuth sulphide and Mn (II) doped bismuth sulphide nanoparticles: characterization and application Cover

Morphologies of nanostructured bismuth sulphide and Mn (II) doped bismuth sulphide nanoparticles: characterization and application

Materials Science-Poland
Volume 35 (2017): Issue 1 (March 2017)
By: Nishant Anasane and  Rakshit Ameta  
Open Access
|Feb 2017

Figures & Tables

XRD patterns of Bi2S3NPS (a) undoped, (b) doped with 5 % Mn ions and (c) doped with 10 % Mn ions.
XRD patterns of Bi2S3NPS (a) undoped, (b) doped with 5 % Mn ions and (c) doped with 10 % Mn ions.
TEM images of Bi2S3NPs (a) undoped, (b) doped with 5 % Mn ions and (c) doped with 10 % Mn ions, (d) and (e) TEM images at higher magnification, (f) ED pattern of Bi2S3NPs.
TEM images of Bi2S3NPs (a) undoped, (b) doped with 5 % Mn ions and (c) doped with 10 % Mn ions, (d) and (e) TEM images at higher magnification, (f) ED pattern of Bi2S3NPs.
HR-SEM images of (a) undoped Bi2S3 NPs, doped with (b) 5 % Mn ions and (c) 10 % Mn ions.
HR-SEM images of (a) undoped Bi2S3 NPs, doped with (b) 5 % Mn ions and (c) 10 % Mn ions.
EDX analysis of Bi2S3NPs (a) undoped and doped with (b) 5 % Mn ions and (c) 10 % Mn ions.
EDX analysis of Bi2S3NPs (a) undoped and doped with (b) 5 % Mn ions and (c) 10 % Mn ions.
FT-IR spectra of (A) Bi2S3NPs, (B) polyoxyethylene 100 sterate.
FT-IR spectra of (A) Bi2S3NPs, (B) polyoxyethylene 100 sterate.
UV-Vis spectra of methyl violet degradation (a) without NPs (b) with Mn doped (5 %) Bi2S3NPs (c) with Mn doped (10 %) Bi2S3NPs.
UV-Vis spectra of methyl violet degradation (a) without NPs (b) with Mn doped (5 %) Bi2S3NPs (c) with Mn doped (10 %) Bi2S3NPs.
UV spectra of redox reaction between Fe(CN)63−${\rm{Fe}}\left( {{\rm{CN}}} \right)_6^{3 - }$ and S2O32−${{\rm{S}}_2}{\rm{O}}_3^{2 - }$ (a) with Mn doped (10 %) Bi2S3NPs, (b) with Mn doped (5 %) Bi2S3NPs, (c) without Bi2S3NPs.
UV spectra of redox reaction between Fe(CN)63−${\rm{Fe}}\left( {{\rm{CN}}} \right)_6^{3 - }$ and S2O32−${{\rm{S}}_2}{\rm{O}}_3^{2 - }$ (a) with Mn doped (10 %) Bi2S3NPs, (b) with Mn doped (5 %) Bi2S3NPs, (c) without Bi2S3NPs.

Percentage Mn (at_%, wt_%) as a dopant in Bi2S3 host determined by EDX, ICP_

Amount of Mn doped [at.%] used in synthesisActual amount of Mn in Bi2S3 matrix (from EDX) [%]Mn/Bi [at.%] determined by ICPMn [wt.%] determined by ICPBi [wt.%] determined by ICP
0––––
53.54.83.6256.24
108.29.39.4750.57
DOI: https://doi.org/10.1515/msp-2017-0032 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 6 - 13
Submitted on: May 7, 2016
Accepted on: Jan 21, 2017
Published on: Feb 24, 2017
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year
Keywords:
nanostructures,
dopant,
metals,
semiconductors,
catalytic properties,
surface properties
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2017 Nishant Anasane, Rakshit Ameta, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

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