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Recovery of the Organic Solvents from the Multicomponent Mixture in the Process of the Fractional Distillation and the Vacuum Distillation Cover

Recovery of the Organic Solvents from the Multicomponent Mixture in the Process of the Fractional Distillation and the Vacuum Distillation

Open Access
|Sep 2024

Abstract

In these times of sustainability, the purification and regeneration of used solvents is attracting a lot of interest for environmental reasons and to reduce production costs. The article presents research on the separation of organic solvents such as acetonitrile, methanol, acetone, and toluene from a multicomponent mixture of liquid organic waste. This is an element of the circular economy and prevents the emission of volatile organic compounds into the environment. In order to separate the mixture and recover the solvents, fractional distillation and vacuum distillation were used together with pre-treatment of the waste using sorption on silica gel and calcium oxide. The analysis of the waste composition and the mixture after the separation was performed by gas chromatography coupled with a mass spectrometer (GC-MS). As a result of the research, the acetonitrile concentration increased to 90.7% after fractional distillation.

DOI: https://doi.org/10.30540/sae-2024-010 | Journal eISSN: 2657-6902 | Journal ISSN: 2081-1500
Language: English
Page range: 111 - 121
Published on: Sep 20, 2024
Published by: Kielce University of Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2024 Anna Ciaciuch, Mariusz Sulewski, published by Kielce University of Technology
This work is licensed under the Creative Commons Attribution 3.0 License.