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Characterization of solvatomorphs of methotrexate using thermoanalytical and other techniques Cover

Characterization of solvatomorphs of methotrexate using thermoanalytical and other techniques

Open Access
|Oct 2009

References

  1. M. C. Tros de Ilarduya, C. Martin, M. M. Goni and M. C. Martinez-Oharriz, Polymorphism of sulindac: Isolation and characterization of a new polymorph and three new solvates,86 (1997) 248-251; DOI: 10.1021/js9601748.
  2. H. G. Brittain, Polymorphism and solvatomorphism 2005,96 (2007) 705-760; DOI: 10.1002/jps.20772.
  3. M. R. Yadav, A. R. Shaikh, V. Ganesan, R. Giridhar and R. Chadha, Studies on the crystal forms of pefloxacin: Preparation, characterization and dissolution profile,97 (2007) 2637-2648; DOI: 10.1002/jps.21178.
  4. E. Swanepoel, W. Liebenberg and M. M. de Villiers, Quality evaluation of generic drugs by dissolution test: changing the USP dissolution medium to distinguish between active and non-active mebendazole polymorphs,55 (2003) 345-349; DOI: 10.1016/S09396411(03)00004-3.
  5. S. Ghodbane and J. A. McCauley, Study of polymorphism of 3-((3-(2-(7-chloro-2-quinolinyl)-(E)-ethenyl)phenyl)((3-(dimethylamino-3-oxopropyl)thio)methyl)-thio) propanoic acid (MK571) by DSC, TG, XRPD and solubility measurements,59 (1990) 281-286; DOI: 10.1016/0378-5173(90)90119-O.
  6. D. Giron, C. Goldbronn, M. Mutz, S. Pfeffer, P. Piechon and P. Schwab, Solid state characterizations of pharmaceutical hydrates,68 (2002) 453-465.
  7. B. K. Saha, A. Nangia and M. Jaskolski, Crystal engineering with hydrogen bonds and halogen bonds,7 (2005) 355-358; DOI: 10.1039/b501693b.
  8. , 34ed., Pharmaceutical Press, London 2005, p. 553.
  9. H. K. Chan and I. Gonda, Methotrexate: Existence of different types of solid,68 (1991) 179-190.
  10. K. Urakami, Characterization of pharmaceutical polymorphs by isothermal calorimetry,6 (2005) 193-203; DOI: 10.2174/1389201054022904.
  11. H. G. Brittain, Spectral methods for the characterization of polymorphs and solvates,86 (1997) 405-412; DOI: 10.1021/js960238e.
  12. D. Giron, Investigations of polymorphism and pseudo-polymorphism in pharmaceuticals by combined thermoanalytical techniques,64 (2001) 37-60.
  13. J. Bauer, J. Morley, S. Spanton, F. J. J. Leusen, R. Henry, S. Hollis, W. Heitmann, A. Mannino, J. Quick and W. Dziki, Identification, preparation and characterization of several polymorphs and solvates of terazosin hydrochloride,95 (2006) 917-928.
  14. G. W. Lu, M. Hawley, M. Smith, B. M. Geiger and W. Pfund, Characterization of a novel polymorphic form of celecoxib,95 (2006) 305-317; DOI: 10.1002/jps.20522.
  15. A. Othman, J. S. O. Evans, I. R. Evans and R. K. Harris, Structural study of polymorphs and solvates of finasteride,96 (2007) 1380-1397; DOI: 10.1002/jps.20940.
  16. M. R. Caira, G. Bettinetti, M. Sorrenti and L. Catenacci, Relationships between structural and thermal properties of anhydrous and solvated crystalline forms of brodimoprim,96 (2007) 996-1007; DOI: 10.1002/jps.20934.
  17. M. Sheikhzadeh, S. Rohani, A. Jutan and T. Manifar, Quantitative and molecular analysis of buspirone hydrochloride polymorphs,96 (2007) 569-583; DOI: 10.1002/jps.20723.
  18. G. D. Christian,, in, 6ed., John Wiley, Singapore 2004, pp. 253-254.
  19. P. Balk and G. C. Benson, Calorimetric determination of the surface enthalpy of potassium chloride,63 (1959) 1009-1012.
  20. USP 27,, USP Convention Inc., Rockville (MD) 2004, pp. 2303-2304.
  21. P. A. Sutton, V. Cody and G. D. Smith, Crystal structure of methotrexate tetrahydrate,108 (1986) 4155-4158; DOI: 10.1021/ja00274a051.
  22. T. W. Hambley, H. K. Chan and I. Gonda, Crystal and molecular structure of methotrexate,108 (1986) 2103-2105; DOI: 10.1021/ja00268a068.
  23. M. R. Caira, G. Bettinetti and M. Sorrenti, Structural relationships, thermal properties and physicochemical characterization of anhydrous and solvated crystalline forms of tetroxoprim,91 (2002) 467-481; DOI: 10.1002/jps.10034.
  24. K. Terada, H. Kitano, Y. Yoshihashi and E. Yonemochi, Quantitative correlation between initial dissolution rate and heat of solution,17 (2008) 920-924.
  25. I. P. Dominic, B. S. Gerald, J. M. Stevenson, S. Lindenbaum, A. W. Douglas, S. D. Klein and J. A. McCauley, High resolution spectroscopic evidence and solution calorimetry studies on the polymorphs of enalapril maleate,28 (1986) 183-191.
DOI: https://doi.org/10.2478/v10007-009-0024-9 | Journal eISSN: 1846-9558 | Journal ISSN: 1330-0075
Language: English, Croatian
Page range: 245 - 257
Published on: Oct 9, 2009
Published by: Croatian Pharmaceutical Society
In partnership with: Paradigm Publishing Services
Related subjects:

© 2009 Renu Chadha, Poonam Arora, Rupinder Kaur, Anupam Saini, Madan Singla, Dharamvir Jain, published by Croatian Pharmaceutical Society
This work is licensed under the Creative Commons License.