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Formation of silicon oxide nanowires in nanomaterial synthesis experiments based on the usage of tube furnace Cover

Formation of silicon oxide nanowires in nanomaterial synthesis experiments based on the usage of tube furnace

Open Access
|Aug 2013

Abstract

In an effort to synthesize doped ZnO nanowires, SiOx nanowires were obtained accidently. In the experiment, mixed powders containing chemicals such as ZnO, graphite, Ga2O3, and In2O3 were placed in the center of a tube furnace, where the temperature was set to 1200 °C and the vacuum was approximately 27 Pa. Silicon wafers were placed around the vicinity of the furnace exit to collect the expected nanomaterials. After prolonged heating, grey layers were found on top of one wafer located inside the furnace. The layer showed no adhesion to the substrate. Characterization by using Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and Energy Dispersive X-ray Spectroscopy (EDS) revealed that this layer consisted of SiOx nanowires. Formation of Si-containing liquid drop and the subsequent growth of SiOx nanowires out of it are suggested as the growth mechanism.

DOI: https://doi.org/10.2478/s13536-013-0111-y | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 350 - 356
Published on: Aug 29, 2013
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2013 Chunfei Li, Virgil Solomon, Marjan Moro, Chad Welsh, Tyler McCauley, Michael Bauer, Joseph Cupo, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.