Have a personal or library account? Click to login
Determination of enantiomeric purity of esomeprazole by capillary electrophoresis Cover

Determination of enantiomeric purity of esomeprazole by capillary electrophoresis

Open Access
|Mar 2021

References

  1. 1. Strand DS, Kim D, Peura DA. 25 Years of Proton Pump Inhibitors: A Comprehensive Review. Gut Liver. 2017 Jan 15;11(1):27–37.10.5009/gnl15502
  2. 2. A proton-pump inhibitor expedition: the case histories of omeprazole and esomeprazole. Nat Rev Drug Discov. 2003 Feb;2(2):132–9.10.1038/nrd1010
  3. 3. Fülöp F, Noszál B, Szász G, Takácsné Novák K. Gyógyszerészi kémia, Semmelweis Kiadó. Budapest; 2010. 455–459.
  4. 4. Roche VF. The Chemically Elegant Proton Pump Inhibitors. Am J Pharm Educ. 2006 Sep;70:101.10.5688/aj7005101
  5. 5. Andersson T, Weidolf L. Stereoselective Disposition of Proton??Pump Inhibitors. Clin Drug Investig. 2008;28:263–79.10.2165/00044011-200828050-00001
  6. 6. Council Of Europe : European Directorate for the Quality of Medicines and Healthcare. European Pharmacopoeia 10.0. Strasbourg; 2019.
  7. 7. United States Pharmacopeial Convention. USP 42 - NF 37 The United States Pharmacopeia and National Formulary 2019.
  8. 8. Bernardo-Bermejo S, Sánchez-López E, Castro-Puyana M, Marina ML. Chiral capillary electrophoresis. TrAC Trends Anal Chem. 2020 Mar 1;124:115807.10.1016/j.trac.2020.115807
  9. 9. Scriba GKE. Chiral recognition in separation science – an update. J Chromatogr A. 2016 Oct;1467:56–78.10.1016/j.chroma.2016.05.061
  10. 10. Scriba GKE. Chiral recognition in separation sciences. Part I: Polysaccharide and cyclodextrin selectors. TrAC Trends Anal Chem. 2019 Nov;120:115639.10.1016/j.trac.2019.115639
  11. 11. Saz JM, Marina ML. Recent advances on the use of cyclodextrins in the chiral analysis of drugs by capillary electrophoresis. J Chromatogr A. 2016 Oct;1467:79–94.10.1016/j.chroma.2016.08.029
  12. 12. Eberle D, Hummel RP, Kuhn R. Chiral resolution of pantoprazole sodium and related sulfoxides by complex formation with bovine serum albumin in capillary electrophoresis. J Chromatogr A. 1997 Jan;759:185–92.10.1016/S0021-9673(96)00769-8
  13. 13. Bonato PS, Paias FO. Enantioselective analysis of omeprazole in pharmaceutical formulations by chiral high-performance liquid chromatography and capillary electrophoresis. J Braz Chem Soc. 2004 Apr;15:318–23.10.1590/S0103-50532004000200025
  14. 14. Nevado JJB, Peñalvo GC, Dorado RMR. Method development and validation for the separation and determination of omeprazole enantiomers in pharmaceutical preparations by capillary electrophoresis. Anal Chim Acta. 2005 Mar;533:127–33.10.1016/j.aca.2004.11.018
  15. 15. Olsson J, Stegander F, Marlin N, Wan H, Blomberg LG. Enantiomeric separation of omeprazole and its metabolite 5-hydroxyomeprazole using non-aqueous capillary electrophoresis. J Chromatogr A. 2006 Oct;1129:291–5.10.1016/j.chroma.2006.07.001
  16. 16. Olsson J, Marlin ND, Blomberg LG. Enantiomeric Separation of Omeperazole Enantiomers by Aqueous CE Using UV and MS Detection. Chromatographia. 2007 Sep 3;66:421–5.10.1365/s10337-007-0317-4
  17. 17. Ma Z, Zhang L, Lin L, Ji P, Guo X. Enantioseparation of rabeprazole and omeprazole by nonaqueous capillary electrophoresis with an ephedrine-based ionic liquid as the chiral selector. Biomed Chromatogr. 2010 Dec;24:1332–7.10.1002/bmc.1445
  18. 18. Guan J, Li H, Yan F, Shi S, Wang S. Optimization and validation of a novel CE method for the enantioseparation of pantoprazole and related benzimididazole using a dual chiral selector system. Electrophoresis. 2014 Oct;35(19):2800–6.10.1002/elps.201400305
  19. 19. Xu Y, Hong T, Chen X, Ji Y. Affinity capilary electrophoresis and fluorescence spectroscopy for studying enantioselective interactions between omeprazole enantiomer and human serum albumin. Electrophoresis. 2017 May;38:1366–73.10.1002/elps.201600375
  20. 20. Estevez P, Flor S, Boscolo O, Tripodi V, Lucangioli S. Development and validation of a capillary electrophoresis method for determination of enantiomeric purity and related substances of esomeprazole in raw material and pellets. Electrophoresis. 2014 Mar;35:804–10.10.1002/elps.201300334
  21. 21. Hancu G, Papp LA, Rusu A. Chiral Separation of the Enantiomers of Omeprazole and Pantoprazole by Capillary Electrophoresis. Chromatographia. 2015 Feb 12;78:279–84.10.1007/s10337-014-2827-1
  22. 22. Wren SAC, Rowe RC. Theoretical aspects of chiral separation in capillary electrophoresis. J Chromatogr A. 1992 Jun;603:235–41.10.1016/0021-9673(92)85366-2
  23. 23. Wren SAC, Rowe RC. Theoretical aspects of chiral separation in capillary electrophoresis. J Chromatogr A. 1992 Sep;609:363–7.10.1016/0021-9673(92)80181-S
  24. 24. Chankvetadze B. Chiral Recognition and Enantioseparation Mechanisms in Capillary Electrokinetic Chromatography. In: Chiral Recognition in Separation Methods. Berlin, Heidelberg:Springer Berlin Heidelberg; 2010. p. 97–152.10.1007/978-3-642-12445-7_5
  25. 25. Scriba GKE. Fundamental aspects of chiral electromigration techniques and application in pharmaceutical and biomedical analysis. J Pharm Biomed Anal. 2011 Jun;55:688–701.10.1016/j.jpba.2010.11.01821131154
  26. 26. Ušelová-Včeláková K, Zusková I, Gaš B. Stability constants of amino acids, peptides, proteins, and other biomolecules determined by CE and related methods: Recapitulation of published data. Electrophoresis. 2007 Jul;28:2145–52.10.1002/elps.20060078017607809
  27. 27. Müllerová L, Dubský P, Gaš B. Twenty years of development of dual and multiselector models in capillary electrophoresis: A review. Electrophoresis. 2014 Oct;35:2688–2700.10.1002/elps.20140014924946108
  28. 28. Dubský P, Dvořák M, Ansorge M. Affinity capillary electrophoresis: the theory of electromigration. Anal Bioanal Chem. 2016 Dec 24;408:8623–41.10.1007/s00216-016-9799-y27558099
  29. 29. Müllerová L, Dubský P, Gaš B. Generalized model of elect-romigration with 1:1 (analyte:selector) complexation stoichiometry: Part II. Application to dual systems and experimental verification. J Chromatogr A. 2015 Mar 6;1384:147–54.10.1016/j.chroma.2015.01.05525666498
  30. 30. Hammitzsch-Wiedemann M, Scriba GKE. Mathematical Approach by a Selectivity Model for Rationalization of pH-and Selector Concentration-Dependent Reversal of the Enantiomer Migration Order in Capillary Electrophoresis. Anal Chem. 2009 Nov;81(21):8765–73.10.1021/ac901160p19810711
  31. 31. Dubský P, Svobodová J, Tesařová E, Gaš B. Enhanced selectivity in CZE multi-chiral selector enantioseparation systems: Proposed separation mechanism. Electrophoresis. 2010 Mar; 31: 1435–41F.10.1002/elps.20090074220358549
DOI: https://doi.org/10.2478/orvtudert-2020-0016 | Journal eISSN: 2537-5059 | Journal ISSN: 1453-0953
Language: English
Page range: 93 - 101
Published on: Mar 30, 2021
Published by: Transylvanian Museum Society
In partnership with: Paradigm Publishing Services
Publication frequency: 2 issues per year

© 2021 Papp Lajos Attila, Hancu Gabriel, Kelemen Hajnal, Gyéresi Árpád, published by Transylvanian Museum Society
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.