Have a personal or library account? Click to login
Determining the Influence of Curing Temperature and SCMs on C-A-S-H Composition Using SEM-EDS Hypermaps Cover

Determining the Influence of Curing Temperature and SCMs on C-A-S-H Composition Using SEM-EDS Hypermaps

Open Access
|Jul 2024

Abstract

Calcium-alumina-silicate-hydrate (C-A-S-H) is the main hydration product formed in Portland composite cement pastes. C-A-S-H is a key phase with regard to the strength and durability of concrete. Proper characterization of C-A-S-H is difficult due to intermixing with other phases, thus limiting the applicability of point scan analyses using scanning electron microscopy (SEM). Recent advances have enabled the use of hypermaps from energy dispersive spectroscopy (EDS) to investigate hydrate phases with better statistics. This study investigated how increased curing temperature and the inclusion of pozzolanic SCMs change the composition of the C-A-S-H, using the edxia plugin and SEM-EDS hypermaps. Composite cement pastes were cured at 20, 38, and 60°C for 180 days before analysis. We discuss the interpretation of the data from hypermaps in comparison to the traditional point scan approach.

DOI: https://doi.org/10.2478/ncr-2024-0006 | Journal eISSN: 2545-2819 | Journal ISSN: 0800-6377
Language: English
Page range: 125 - 146
Submitted on: Apr 2, 2024
Accepted on: Jun 24, 2024
Published on: Jul 5, 2024
Published by: Nordic Concrete Federation
In partnership with: Paradigm Publishing Services
Publication frequency: 2 issues per year

© 2024 Petter Hemstad, Petter Kjellemyr, Klaartje De Weerdt, published by Nordic Concrete Federation
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.