Synthesis of nano Mn-Zn ferrites by gel combustion method with three different fuels and investigation of their structure and properties

Nima Vahdati; Arman Sedghi

doi:10.2478/msp-2020-0037

Abstract

The purpose of studying the properties of zinc-manganese nanoferrite was to compare organic fuels that were produced in conditions created by the auto gel combustion method, using citric acid, glycine, and urea with different pH values: (citric acid = 6, glycine = 3 and urea = 0). The samples were prepared in stoichiometric ratios to gain Mn_0.5Zn_0.5Fe₂O₄, and all the samples were calcined in the same condition (500 °C and 30 minutes). It should be noted that the entire process of synthesis was photographed to analyze the effect of fuels during the combustion process. Combustion reactions were studied by simultaneous thermal analysis (STA), FT-IR spectroscopy, and X-ray diffraction (XRD), also the Rietveld method was used to determine the type and amount of crystalline phases. Magnetic properties of the samples were measured by vibration sample magnetometer (VSM), and their morphology and powder agglomeration was observed by field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). Superior magnetic properties of the sample synthesized with glycine were achieved. Urea gave the smallest particle size, while citric acid produced intermediate properties.

References

[1] Seyyed Ebrahimi S.A., Masoudpanah S.M., J. Magn. Magn. Mater, (2014), 77.10.1016/j.jmmm.2014.01.017
Search in Google Scholar Back to article
[2] Gimenes R., Baldissera M.R., da Silva M.R.A., da Silveira C.A., Soares D.A.W., Perazolli L.A., da Silva M.R., Zaghete M.A., Ceram. Int, 1 (2012), 741.
Search in Google Scholar Back to article
[3] Sutka Andris., Mezinskis Gundars., Front. Mater. Sci, 2 (2012), 128.10.1007/s11706-012-0167-3
Search in Google Scholar Back to article
[4] Ghobeiti Hasab M., Ebrahimi S.A., Badiei A., J. Non.-Cryst. Solids, 8-10 (2007), 814.10.1016/j.jnoncrysol.2006.12.048
Search in Google Scholar Back to article
[5] Murugesan C., Mdgazzali P.M., Chandrasekaran G., J. Mater. Sci.-Mater. El, 8 (2013), 3136.10.1007/s10854-013-1222-2
Search in Google Scholar Back to article
[6] Hajarpour S., Gheisari KH., Honarbakhsh Raouf A., J. Magn. Magn. Mater, 329 (2013), 165.10.1016/j.jmmm.2012.10.023
Search in Google Scholar Back to article
[7] Tonoilo J.C., Lima M.D., Takimi A.S., Bergmann C.P., Mater. Res. Bull, 3 (2005), 561.10.1016/j.materresbull.2004.07.019
Search in Google Scholar Back to article
[8] Vasanthi V., Shanmugavani A., Sanjeeviraja C., Kalai Selvan R., J. Magn. Magn. Mater, 13 (2012), 2100.10.1016/j.jmmm.2012.02.018
Search in Google Scholar Back to article
[9] Hwang C.C., Tsai J.S., Huang T.H., Mater. Chem. Phys, 2-3 (2005), 330.10.1016/j.matchemphys.2005.03.056
Search in Google Scholar Back to article
[10] Pedzich Z., Bucko M.M., Krolikowski M., Bakalarska M., Babiarz J., J. Eur. Ceram. Soc, 6 (2004), 1053.10.1016/S0955-2219(03)00386-8
Search in Google Scholar Back to article
[11] Hou J.G., Qu Y.F., Ma W.B., Sun Q.C., J. Sol.-Gel. Sci. Techn, 1 (2007), 15.10.1007/s10971-007-1600-4
Search in Google Scholar Back to article
[12] Bakhshi H., Shokuhfar A., Seyyed Afghahi S.S., Ceram. Int, 9 (2015), 10736.10.1016/j.ceramint.2015.05.009
Search in Google Scholar Back to article
[13] Motevalian A., Salem S., Particuology, (2016), 108.10.1016/j.partic.2015.03.005
Search in Google Scholar Back to article
[14] Mohamed R.M., Rashad M.M., Haraz F., Sigmund W., J. Magn. Magn. Mater, 14 (2010), 2058.10.1016/j.jmmm.2010.01.034
Search in Google Scholar Back to article
[15] Rasly M., Rashad M.M., J. Magn. Magn. Mater, (2013), 58.10.1016/j.jmmm.2013.02.038
Search in Google Scholar Back to article
[16] Rashad M.M., Turky A.O., Kandil A.T., J. Mater. Sci.-Mater. El, 9 (2013) 3284.10.1007/s10854-013-1244-9
Search in Google Scholar Back to article
[17] Rashad M.M., J. Mater. Sci.-Mater. El, 4 (2012), 882.10.1007/s10854-011-0513-8
Search in Google Scholar Back to article
[18] Bahadur D., Rajakumar S., Kumar A., J. Chem. Sci, 1 (2006), 15.10.1007/BF02708761
Search in Google Scholar Back to article
[19] Abu el Fadl A., Hassan A.M., Mahmoud M.H., Tatarchuk T., Yaremiy I.P., Gismelssed A.M., Ahmed M.A., J. Magn. Magn. Mater, (2019), 192.
Search in Google Scholar Back to article
[20] Ahmed M.A., Hassan H.E., Eltabey M.M., Latla K., Tatarchuk T.R., Physica. B, (2018), 195.
Search in Google Scholar Back to article
[21] Rajesh Babu B., Tatarchuk T., Mater. Chem. Phys, (2018) 534.10.1016/j.matchemphys.2017.12.084
Search in Google Scholar Back to article
[22] Kane S.N., Raghuvanshi S., Satalkar M., Reddy V.R., Deshpande U.P., Tatarchuk T.R., Mazaleyrat F., AIP. Conf. Proc, 1 (2018), 030089.
Search in Google Scholar Back to article
[23] Tatarchuk Tetiana., Bououdina M., Judith Vijaya J., John Kennedy L., Nanophysics, Nanomaterials, Interface Studies, and Applications, Springer, Lviv, 2016.
Search in Google Scholar Back to article
[24] Hu P., Yang H.B., Pan D.A., Wang H., Tian J.J., Zhang S.G., Wang X.F., A.Volinsky A., J. Magn. Magn. Mater, 1 (2010) 173.
Search in Google Scholar Back to article
[25] Bakhshi H., Shokuhfar A., Vahdati N., Int. j. Min. Met. Mater, 9 (2016), 1104.10.1007/s12613-016-1328-7
Search in Google Scholar Back to article
[26] Waqas H., Qureshi A.H., J. Therm. Anal. Calorim, 2 (2009), 355.10.1007/s10973-009-0289-8
Search in Google Scholar Back to article
[27] Costa A.C.F.M, Morelli M.R., Kiminami R.H., J. Mater. Synth. Process, 6 (2001), 347.10.1023/A:1016356623401
Search in Google Scholar Back to article
[28] Costa A.C.F.M., Silva V.J., Xin C.C., Viera D.A., Cornejo D.R., Kiminami R.H.G.A., J. Alloy. Compd, 2 (2010), 503.10.1016/j.jallcom.2009.10.065
Search in Google Scholar Back to article
[29] Tatarchuk T.R., Bououdina M., Paliychuk N.D., Yaremiy I.P., Moklyak V.V., J. Alloy. Compd, (2017), 777.10.1016/j.jallcom.2016.10.067
Search in Google Scholar Back to article
[30] Tatarchuk T.R., Paliychuk N.D., Bououdina M., Al Najar B., Pacia M., Macyk W., Shyichunk A., J. Alloy. Compd, (2018), 1256.10.1016/j.jallcom.2017.10.103
Search in Google Scholar Back to article
[31] Szczygiel I., Winiarska K., Bien Ko A., Suracka K., Gaworska Koniarek D., J. Alloy. Compd, (2014), 1.10.1016/j.jallcom.2014.03.109
Search in Google Scholar Back to article
[32] Maensiri S., Chivalrat M., Boonchom B., Seraphin Supapan., Scripta. Mater, 9 (2007), 797.10.1016/j.scriptamat.2006.09.033
Search in Google Scholar Back to article
[33] Gabal M.A., Abdel Daiem A.M., Al Angari Y.M., Ismail I.M., Polyhedron, (2013), 105.10.1016/j.poly.2013.04.027
Search in Google Scholar Back to article
[34] Wang W., Zang C., Jiao Q., J. Magn. Magn. Mater, (2014), 116.10.1016/j.jmmm.2013.08.057
Search in Google Scholar Back to article

Synthesis of nano Mn-Zn ferrites by gel combustion method with three different fuels and investigation of their structure and properties

Abstract

Paradigm

My account