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Fig S1.

Fig S4.

Dose recovery ratios and residual doses for IR and pIRIR measured on all samples from the Bee pit and the Velická dolina valley_
| Sample no. | IR50 | pIRIR225 | ||||||
|---|---|---|---|---|---|---|---|---|
| Dose recovery ratio | Error | Residual | Error | Dose recovery ratio | Error | Residual | Error | |
| 19082 | 0.89 | 0.03 | 2.73 | 0.2 | 0.92 | 0.03 | 16.09 | 0.12 |
| 19083 | 0.84 | 0.03 | 2.56 | 0.1 | 0.89 | 0.03 | 15 | 0.1 |
| 19086 | 0.86 | 0.03 | 3.29 | 0.1 | 0.87 | 0.03 | 17.3 | 0.1 |
| 19087 | 0.84 | 0.03 | 2.64 | 0.1 | 0.9 | 0.03 | 17.5 | 0.1 |
| 19091 | 0.84 | 0.03 | 2.73 | 0.1 | 0.92 | 0.03 | 15.6 | 0.5 |
| 19092 | 0.88 | 0.03 | - | - | 0.91 | 0.03 | - | - |
| 19094 | 0.92 | 0.03 | 2.89 | 0.3 | 0.94 | 0.03 | 15.5 | 1.6 |
| 19096 | - | - | 2.86 | 0.2 | - | - | 15.3 | 1.5 |
Results of the SOL2 bleaching experiment for sample 19087_
| Bleaching time (min) | IR50 De (Gy) | IR50 Ln/Tn | pIRIR225 De (Gy) | pIRIR225 Ln/Tn |
|---|---|---|---|---|
| 0 (Natural) | 232.8 ± 2.8 | 6.49 ± 0.08 | 587.8 ± 19.4 | 8.88 ± 0.39 |
| 1 | 45.4 ± 8.7 | 1.55 ± 0.27 | 311.7 ± 31.7 | 7.38 ± 0.52 |
| 5 | 6.8 ± 0.3 | 0.24 ± 0.01 | 92.7 ± 4.4 | 3.04 ± 0.12 |
| 20 | 3.3 ± 0.2 | 0.12 ± 0.01 | 29.5 ± 0.7 | 1.06 ± 0.02 |
| 60 | 2.2 ± 0.1 | 0.08 ± 0.00 | 16.3 ± 0.7 | 0.60 ± 0.03 |
| 20160 | 0.5 ± 0.0 | 0.02 ± 0.00 | 4.8 ± 0.3 | 0.17 ± 0.01 |
Results of the IR50 and pIRIR225 measurements: g-values, feldspar dose estimates, the number aliquots with De < 2D0 compared to the total number of accepted aliquots and the uncorrected and corrected ages_
| Sample No. | Unit / Site No. | g-value (%/decade) | De (Gy) | Accepted (De<2D0) / Total aliquots | Uncorrected age (ka) | Corrected age (ka) | |||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| IR50 | pIRIR225 | IR50 | pIRIR225 | IR50 | pIRIR225 | IR50 | pIRIR225 | IR50 | pIRIR225 | ||
| 19082 | Unit 3 | 6.71 ± 0.1 | 2.23 ± 0.3 | 414 ± 15 | 868 ± 86 | 12(12)/12 | 12(1)/12 | 125 ± 7.8 | 261 ± 29 | 278 ± 18 | 326 ± 38 |
| 19083 | Unit 1B | 4.82 ± 0.7 | 1.56 ± 0.1 | 351 ± 14 | 844 ± 116 | 12(12)/12 | 12(1)/12 | 109 ± 7.2 | 263 ± 39 | 185 ± 28 | 308 ± 51 |
| 19084 | Unit 3 | 9.83 ± 0.2 | 2.84 ± 0.2 | 348 ± 14 | 741 ± 80 | 12(12)/12 | 12(2)/12 | 129 ± 8.7 | 275 ± 33 | 624 ± 82 | 368 ± 46 |
| 19085 | Unit 3 | 6.52 ± 0.1 | 1.66 ± 0.6 | 317 ± 11 | 760 ± 76 | 12(12)/12 | 12(1)/12 | 106 ± 6.8 | 254 ± 29 | 230 ± 16 | 300 ± 39 |
| 19086 | Unit 3 | 1.66 ± 0.2 | 0.09 ± 0.1 | 387 ± 16 | 812 ± 105 | 12(12)/12 | 12(0)/12 | 100 ± 7.3 | 210 ± 30 | 117 ± 8.7 | 212 ± 29 |
| 19087 | Unit 12 | 5.06 ± 0.3 | 1.48 ± 0.1 | 351 ± 13 | 788 ± 73 | 12(12)/12 | 12(2)/12 | 120 ± 7.6 | 269 ± 29 | 208 ± 16 | 311 ± 31 |
| 19088 | Unit 12 | 5.85 ± 0.2 | 0.81 ± 0.6 | 326 ± 11 | 776 ± 74 | 12(12)/12 | 12(1)/12 | 81 ± 4.9 | 193 ± 21 | 156 ± 12 | 208 ± 27 |
| 19089 | Unit 12 | 5.05 ± 0.02 | 1.99 ± 0.02 | 372 ± 14 | 850 ± 91 | 12(12)/12 | 12(2)/12 | 109 ± 6.6 | 249 ± 29 | 188 ± 11 | 304 ± 36 |
| 19090 | Unit 9 | 5.71 ± 0.4 | 2.16 ± 0.1 | 354 ± 13 | 763 ± 73 | 12(12)/12 | 12(1)/12 | 115 ± 7.8 | 248 ± 28 | 219 ± 22 | 308 ± 31 |
| 19091 | Unit 9 | 8.69 ± 1.1 | 0.37 ± 0.4 | 360 ± 13 | 710 ± 58 | 30(30)/30 | 30(8)/30 | 97.3 ± 5.7 | 192 ± 18 | 318 ± 185 | 199 ± 19 |
| 19092 | Unit 5 | 5.26 ± 0.3 | 0.70 ± 0.4 | 465 ± 20 | 949 ± 123 | 12(12)/12 | 12(2)/12 | 132 ± 8.6 | 269 ± 38 | 236 ± 19 | 287 ± 39 |
| 19093 | Site 1 | 8.01 ± 0.6 | 1.05 ± 0.3 | 338 ± 15 | 636 ± 64 | 12(12)/12 | 12(5)/12 | 79.5 ± 5.5 | 150 ± 17 | 219 ± 50 | 165 ± 19 |
| 19094 | Site 1 | 9.43 ± 0.5 | 3.04 ± 0.1 | 304 ± 14 | 611 ± 49 | 12(11)/15 | 12(7)/13 | 69.9 ± 5.2 | 139 ± 14 | 266 ± 105 | 188 ± 21 |
| 19095 | Site 1 | 4.83 ± 0.3 | 2.06 ± 0.2 | 325 ± 13 | 709 ± 85 | 12(12)/12 | 12(5)/13 | 86.1 ± 5.9 | 188 ± 25 | 145 ± 12 | 231 ± 29 |
| 19096 | Site 2 | 7.20 ± 0.6 | 1.52 ± 0.2 | 346 ± 14 | 770 ± 72 | 29(29)/30 | 29(9)/30 | 90.9 ± 6.1 | 202 ± 22 | 204.5 ± 34 | 234 ± 24 |
| 19097 | Site 2 | 7.25 ± 1.1 | −0.41 ± 0.1 | 330 ± 12 | 798 ± 88 | 12(12)/15 | 12(3)/18 | 96.7 ± 6.9 | 234 ± 30 | 234 ± 83 | * |
| 19098 | Site 3 | 8.61 ± 0.8 | 3.31 ± 0.2 | 134 ± 4.2 | 361 ± 22 | 12(12)/12 | 12(10)/12 | 38.5 ± 2.9 | 103 ± 9.5 | 116 ± 35 | 145 ± 14 |
| 19100 | Site 4 | 4.56 ± 0.6 | 1.43 ± 0.2 | 306 ± 15 | 839 ± 122 | 12(12)/12 | 12(2)/12 | 81.7 ± 6.1 | 224 ± 35 | 130 ± 14 | 257 ± 41 |
| 19101 | Site 5 | 11.49 ± 0.3 | 1.65 ± 0.2 | 131 ± 4.1 | 506 ± 37 | 12(12)/14 | 12(7)/12 | 37.7 ± 2.8 | 146 ± 14 | 307 ± 118 | 172 ± 17 |
| 19102 | Site 5 | 7.49 ± 0.9 | 2.60 ± 0.2 | 96.0 ± 3.1 | 387 ± 32 | 33(33)/33 | 33(22)/35 | 29.1 ± 2.0 | 117 ± 12 | 69 ± 15 | 152 ± 15 |
| 19105 | Site 6 | 10.77 ± 1.0 | 2.98 ± 0.3 | 31.5 ± 1.5 | 109 ± 7.0 | 12(12)/15 | 12(9)/18 | 17.7 ± 1.6 | 61.6 ± 6.3 | 79 ± 37 | 82 ± 10 |
| 19106 | Site 6 | 6.74 ± 0.04 | 1.64 ± 0.1 | 56.2 ± 1.9 | 183 ± 5.8 | 12(12)/15 | 12(9)/18 | 20.1 ± 1.6 | 65.4 ± 5.2 | 42 ± 3.5 | 77 ± 5.7 |
| 20026 | Site 2 | 5.42 ± 0.41 | 0.66 ± 0.25 | 453 ± 10 | 737 ± 47 | 5(5)/5 | 5(5)/5 | n/a | n/a | n/a | n/a |
| 20028 | Site 8 | 4.89 ± 0.83 | 0.88 ± 0.41 | 18.4 ± 3.9 | 55.6 ± 5.6 | 12(12)/12 | 12(12)/12 | 5.0 ± 1.1 | 15.0 ± 1.7 | 7.6 ± 2.0 | 16.1 ± 1.9 |
The water content values used for the age calculation, per sample_ For three samples the uncorrected pIRIR age (ka) is shown calculated with all three water contents_
| Sample No. | Field Water Content (%) | Saturated Water Content (%) | Expected Water Content (%) |
|---|---|---|---|
| 19082 | 11 | 31 | 27 |
| 19083 | 15 | 25 | 24 |
| 19084 | 7 | 22 | 19 |
| 19085 | 13 | 25 | 23 |
| 19086 | 21 | 27 | 26 |
| 19087 | 24 | 35 | 29 |
| 19088 | 23 | 30 | 26 |
| 19089 | 15 | 27 | 20 |
| 19090 | 15 | 35 | 29 |
| 19091 | 17 | 31 | 27 |
| 19092 | 32 | 38 | 36 |
| 19093 | 16 | 25 | 21 |
| 19094 | 9 | 22 | 13 |
| 19095 | 18 | 28 | 21 |
| 19096 | 28 | 35 | 31 |
| 19097 | 28 | 35 | 31 |
| 19098 | 5 | 23 | 23 |
| 19099 | 5 | 23 | 23 |
| 19100 | 8 | 29 | 23 |
| 19101 | 17 | 31 | 30 |
| 19102 | 21 | 30 | 29 |
| 19105 | 19 | 49 | 49 |
| 19106 | 19 | 49 | 49 |
| 20028 | 0 | 18 | 15 |
OSL parameters calculated from the quartz extracts using linear modulation compared to other values from literature_
| Sample | OSL component | Detraping probability (b) | Photoionisation cross-section (ϭ) | Relative Cross-section |
|---|---|---|---|---|
| 19082 | Fast | 22.4 ± 4.9 | 1.4 × 10−16 | 1 |
| Slow1 | 1.8 ± 0.2 | 1.2 × 10−17 | 0.09 | |
| Slow2 | 0.17 ± 0.003 | 1.1 × 10−18 | 0.01 | |
| Slow3 | 0.018 ± 0.004 | 1.1 × 10−19 | 0.001 | |
| Slow4 | 0.0004 ± 0.0003 | 2.5 × 10−20 | 0.0002 | |
| 19095 | Fast | 9.6 ± 3.2 | 6.1 × 10−17 | 1 |
| Medium | 0.94 ± 0.1 | 6.0 × 10−18 | 0.1 | |
| Slow2 | 0.12 ± 0.008 | 7.8 × 10−19 | 0.01 | |
| Slow3 | 0.017 ± 0.0008 | 1.2 × 10−19 | 0.002 | |
| Slow4 | 0.004 ± 0.00009 | 2.9 × 10−20 | 0.0006 | |
| 19104 | Fast | 1.6 ± 0.3 | 6.2 × 10−18 | 1 |
| Slow1 | 0.08 ± 0.04 | 5.0 × 10−19 | 0.05 | |
| Slow3 | 0.005 ± 0.0003 | 3.1 × 10−20 | 0.003 | |
| Calib. quartz | Fast | 2.7 ± 0.09 | 1.6 × 10−17 | 1 |
| Slow4 | 0.0007 ± 0.00003 | 4.5 × 10−21 | 0.0003 | |
| Jain et al. (2003) | Fast | 2.5 ± 0.2 | 2.3 × 10−17 | 1 |
| Medium | 0.62 ± 0.05 | 5.6 × 10−18 | 0.2 | |
| Slow1 | 0.15 ± 0.03 | 1.3 × 10−18 | 0.06 | |
| Slow2 | 0.023 ± 0.005 | 2.1 × 10−19 | 0.01 | |
| Slow3 | 0.0022 ± 0.0002 | 2.1 × 10−20 | 0.001 | |
| Slow4 | 0.00030 ± 0.00001 | 2.8 × 10−21 | 0.0001 | |
| Durcan and Duller (2011) | Fast | n.a. | 2.6 × 10−17 | 1 |
| Medium | n.a. | 4.3 × 10−18 | 0.16 | |
| Slow1 | n.a. | 1.1 × 10−18 | 0.04 | |
| Slow2 | n.a. | 3.0 × 10−19 | 0.01 | |
| Slow3 | n.a. | 3.4 × 10−20 | 0.001 | |
| Slow4 | n.a. | 9.1 × 10−21 | 0.0003 | |
OSL doses, dose rates and ages for the quartz samples_
| Sample No. | Number of aliquots | Type of OSL measurement | Mean Dose ± error (Gy) | Total Dose rate ± error (Gy ka−1) | Age (ka) |
|---|---|---|---|---|---|
| 19082 | 18 | Differential OSL | 268 ± 58 | 2.6 ± 0.1 | 104 ± 23 |
| 12 | Pulsed OSL | 102 ± 6 | 40 ± 3 | ||
| 19083 | 3 | Standard SAR | 143 ± 27 | 2.7 ± 0.1 | 53 ± 10 |
| 19084 | 6 | Standard SAR | 160 ± 41 | 2.1 ± 0.1 | 77 ± 20 |
| 19085 | 3 | Standard SAR | 103 ± 21 | 2.4 ± 0.1 | 42 ± 9 |
| 19090 | 3 | Standard SAR | 96 ± 11 | 2.6 ± 0.1 | 38 ± 5 |
| 19091 | 3 | Standard SAR | 186 ± 55 | 3.2 ± 0.1 | 58 ± 17 |
| 19092 | 3 | Standard SAR | 114 ± 40 | 3.3 ± 0.2 | 35 ± 12 |
| 19102 | 12 | Pulsed OSL | 30 ± 6 | 2.3 ± 0.2 | 13 ± 3 |
Concentration of radioactive elements in the sampled sediments (from gamma spectrometry) and the dose rate from cosmic radiation to each sample (as calculated in DRAC v1_2 (Durcan et al_, 2015))_
| Sample No. | U (ppm) ± error | Th (ppm) ± error | K (%) ± error | Cosmic dose rate (Gy. ka−1) | Total Dose Rate (Gy. ka−1) | wce(%) |
|---|---|---|---|---|---|---|
| 19082 | 1.49 ± 0.58 | 5.87 ± 0.15 | 2.52 ± 0.04 | 0.14 ± 0.01 | 3.33 ± 0.17 | 27 |
| 19083 | 0.96 ± 0.45 | 6.55 ± 0.13 | 2.42 ± 0.05 | 0.10 ± 0.01 | 3.21 ± 0.16 | 24 |
| 19084 | 0.48 ± 0.17 | 4.98 ± 0.08 | 1.91 ± 0.03 | 0.07 ± 0.01 | 2.70 ± 0.15 | 19 |
| 19085 | 0.92 ± 0.54 | 5.11 ± 0.14 | 2.23 ± 0.04 | 0.10 ± 0.01 | 2.99 ± 0.16 | 23 |
| 19086 | 2.43 ± 1.24 | 8.48 ± 0.33 | 2.86 ± 0.10 | 0.09 ± 0.01 | 3.87 ± 0.23 | 26 |
| 19087 | 1.22 ± 0.42 | 6.96 ± 0.12 | 1.99 ± 0.04 | 0.16 ± 0.02 | 2.93 ± 0.15 | 29 |
| 19088 | 4.23 ± 0.84 | 9.35 ± 0.23 | 2.46 ± 0.05 | 0.17 ± 0.02 | 4.03 ± 0.20 | 26 |
| 19089 | 1.04 ± 0.21 | 5.60 ± 0.08 | 2.52 ± 0.03 | 0.17 ± 0.02 | 3.41 ± 0.16 | 20 |
| 19090 | 0.74 ± 0.71 | 5.97 ± 0.18 | 2.32 ± 0.05 | 0.21 ± 0.02 | 3.07 ± 0.17 | 29 |
| 19091 | 2.08 ± 0.39 | 8.79 ± 0.11 | 2.59 ± 0.03 | 0.21 ± 0.02 | 3.70 ± 0.17 | 27 |
| 19092 | 2.20 ± 0.79 | 7.27 ± 0.21 | 2.74 ± 0.05 | 0.20 ± 0.02 | 3.53 ± 0.18 | 36 |
| 19093 | 3.28 ± 0.34 | 12.0 ± 0.17 | 2.56 ± 0.04 | 0.20 ± 0.02 | 4.24 ± 0.23 | 21 |
| 19094 | 2.85 ± 0.64 | 12.3 ± 0.19 | 2.48 ± 0.05 | 0.19 ± 0.02 | 4.39 ± 0.26 | 13 |
| 19095 | 2.38 ± 0.45 | 10.6 ± 0.13 | 2.29 ± 0.03 | 0.19 ± 0.02 | 3.78 ± 0.21 | 21 |
| 19096 | 3.60 ± 0.44 | 11.6 ± 0.12 | 2.47 ± 0.04 | 0.06 ± 0.01 | 3.80 ± 0.20 | 31 |
| 19097 | 1.61 ± 0.86 | 13.5 ± 0.24 | 2.21 ± 0.05 | 0.11 ± 0.01 | 3.41 ± 0.21 | 31 |
| 19098 | 1.15 ± 0.49 | 6.80 ± 0.14 | 2.18 ± 0.05 | 0.27 ± 0.03 | 3.48 ± 0.23 | 23 |
| 19100 | 2.94 ± 0.58 | 12.1 ± 0.17 | 2.09 ± 0.05 | 0.17 ± 0.02 | 3.75 ± 0.21 | 23 |
| 19101 | 2.39 ± 0.60 | 11.8 ± 0.17 | 2.32 ± 0.05 | 0.18 ± 0.02 | 3.48 ± 0.23 | 30 |
| 19102 | 1.39 ± 0.72 | 8.57 ± 0.19 | 2.31 ± 0.05 | 0.17 ± 0.02 | 3.29 ± 0.20 | 29 |
| 19104 | 1.50 ± 0.25 | 6.53 ± 0.07 | 1.81 ± 0.03 | 0.29 ± 0.03 | 2.43 ± 0.20 | - |
| 19105 | 1.06 ± 0.30 | 6.68 ± 0.15 | 1.89 ± 0.04 | 0 (surface) | 1.78 ± 0.14 | - |
| 19106 | 1.06 ± 0.30 | 6.68 ± 0.15 | 1.89 ± 0.04 | 0.31 ± 0.03 | 2.80 ± 0.20 | 49 |
| 20028 | 1.18 ± 0.27 | 10.16 ± 0.15 | 2.44 ± 0.04 | 0.15 ± 0.02 | 3.72 ± 0.17 | 15 |
Sample information acquired from the investigated study areas_ Lithofacies codes are based on Krüger and Kjaer (1999)_
| Sample No. | Site | UTM 33N easting | UTM 33N northing | Location / Sample type | Depth in m (overburden sediment) | Stratigraphic unit | Lithofacies | Fraction (μm) |
|---|---|---|---|---|---|---|---|---|
| 19082 | Bee Pit | 42829 | 5439202 | Lower section | 7.1 | B3 | SiSm(ng) | 180–250 |
| 19083 | Bee Pit | 428289 | 5439024 | Lower section | 11.4 | B1B | SSim | 180–250 |
| 19084 | Bee Pit | 428292 | 5439015 | Lower section | 13.8 | B3 | SiSm(ng) | 180–250 |
| 19085 | Bee Pit | 428289 | 5439024 | Lower section | 11.4 | B3 | SiSm(ng) | 180–250 |
| 19086 | Bee Pit | 428283 | 5439047 | Lower section | 10.8 | B3 | SiSm(ng) | 180–250 |
| 19087 | Bee Pit | 428228 | 5438971 | Upper section | 5.4 | B12 | SiSm(ng) | 180–250 |
| 19088 | Bee Pit | 428228 | 5438971 | Upper section | 5.4 | B12 | SiSm(ng) | 180–250 |
| 19089 | Bee Pit | 428228 | 5438971 | Upper section | 5.4 | B12 | Sm(ng) | 180–250 |
| 19090 | Bee Pit | 428282 | 5439016 | Lower section | 2.2 | B9 | SiSm | 180–250 |
| 19091 | Bee Pit | 428282 | 5439016 | Lower section | 2.2 | B9 | SiSm | 180–250 |
| 19092 | Bee Pit | 428286 | 5439018 | Lower section | 3.6 | B5 | Sm(ng) | 180–250 |
| 19093 | GYW, site 1 | 439489 | 5441932 | GYW South (YS) | 1.8 | YS3 | GSm | 180–250 |
| 19094 | GYW, site 1 | 439489 | 5441932 | GYW South (YS) | 1.7 | YS3 | Sm | 180–250 |
| 19095 | GYW, site 1 | 439489 | 5441932 | GYW South (YS) | 2.2 | YS3 | GSm | 180–250 |
| 19096 | GYW, site 2 | 439514 | 5442023 | GYW North (YN) | 15 | YN1 | Sm | 180–250 |
| 19097 | GYW, site 2 | 439514 | 5442023 | GYW North (YN) | 15 | YN1 | Sm | 180–250 |
| 19098 | Site 3 | 439737 | 5441549 | Flood deposit | 0.24 | - | Gm | 250–355 |
| 19099* | Site 4 | 439677 | 5441615 | East of Velická potok | 2 | - | Gm | * |
| 19100 | Site 4 | 439677 | 5441615 | East of Velická potok | 2.5 | - | Sm | 180–250 |
| 19101 | Site 5 | 439605 | 5441701 | West of Velická potok | 2.6 | - | Sh | 90–180 |
| 19102 | Site 5 | 439605 | 5441701 | West of Velická potok | 2.5 | - | Sh | 180–250 |
| 19105 | Site 6 | 439775 | 5441345 | Modern Analogue (MA) | 0 | - | Sm | 180–250 |
| 19106 | Site 6 | 439775 | 5441345 | Modern Analogue (MA) | 0.03 | - | Sm | 250–355 |
| 19103* | Site 7 | 440614 | 5436964 | Distant MA | 0 | - | Sm | * |
| 19104* | Site 7 | 440614 | 5436964 | Distant MA | 0.12 | - | Sm | 90–180 |
| 20026 | GYW, site 2 | 439514 | 5442023 | Saturated sample | 15 | YN1 | Boulder | 180–250 |
| 20028 | Site 8 | 439819 | 5442867 | Moraine | 5 | - | DmC | 180–250 |
Water content test, where ages for samples 19084, 19086 and 19094 were calculated for 0% and 50% water content_
| Sample No. | Water Content (0%) | Water Content (50%) | Expected Water Content |
|---|---|---|---|
| Age (ka) | Age (ka) | Age (ka) | |
| 19084 | 236 ± 28 | 328 ± 40 | 275 ± 33 |
| 19086 | 169 ± 24 | 245 ± 35 | 210 ± 30 |
| 19094 | 123 ± 13 | 178 ± 17 | 139 ± 14 |