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Component-Resolved Analysis Towards Correlation between Thermoluminescence and Optically Stimulated Luminescence in Commercial Magnesium Oxide Cover

Component-Resolved Analysis Towards Correlation between Thermoluminescence and Optically Stimulated Luminescence in Commercial Magnesium Oxide

Open Access
|Dec 2021

Figures & Tables

Fig. 1

CW-OSL decay curves received at room temperature, using blue light for stimulation times 128, 256, 512, 1024 and 2048 s, which coincide. This experimental feature yields the excellent reproducibility the measuring sequence.

Fig. 2

Shapes of the R-TL glow-curves received after bleaching with blue light for all stimulation times, ranging between 1 and 2048 s.

Fig. 3

Shapes of the LM-OSL curves received at RT and at 170°C after a pre-heat at 180°C.

Fig. 4

The ratio of integrated CW-OSL over the TL-lost during the various stimulation times. The TL-lost is defined as the difference between the total integrals of the un-bleached glow-curve minus the bleached TL glow-curves (a) For OSL measured at RT and (b) for OSL measured at 170°C.

Fig. 5

Results of the CGCD analysis of RTL glow-curves after CWOSL at RT using Eqs. 3.5 and 3.6. The open circles represent the experimental glow-curve after CW-OSL for 1 s. The line through the experimental points is the fitting line. The continuous lines present the results of the CGCD of all R-TL glow-curves of Fig. 2 without the repeating of the experimental curves. The results for fitting parameters are listed in Table 1.

Fig. 6

Analysis examples of R-TL decay curves based on the integrated signal of the main R-TL glow-peaks resulted from CGCD analysis shown individually in Fig.5. The fit was performed using Eqs. 3.1 and 3.4. The results of the fitting parameters are listed in Table 2.

Fig. 7

Component resolved of LM-OSL curves received at RT and at 170°C after a pre-heat at 180°C, using Eqs. 3.8 and 3.9. The results of the fitting parameters are listed in Table 3.

The values of the trapping parameters of MgO resulting from the CGCD analysis using both general order kinetics and OTOR analytical equation_

Peak no.Tm (°C)E (eV)Rb%OSL (RT)%OSL (170°C)
1102 ± 20.90 ± 0.090.42 ± 0.071.40 ± 0.0212.50-
2132 ± 10.94 ± 0.110.76 ± 0.171.97 ± 0.051.50-
3194 ± 20.82 ± 0.030.90 ± 0.061.55 ± 0.051.551.30
4292 ± 41.13 ± 0.050.65 ± 0.161.60 ± 0.1038.1250.44
5353 ± 31.24 ± 0.030.81 ± 0.041.90 ± 0.0730.6432.94
6464 ± 21.45 ± 0.040.71 ± 0.071.79 ± 0.1715.2714.59

The fitting parameters of the RTL integrated signals as a function of the bleaching time using both general order and OTOR analytical equations_ The values are the mean between of the values obtained by the two different equations_ The error values provide a strong indication towards the agreement of the two different Equations used_

Peak Tm (°C)OSL Tτ1 (s)%τ2 (s)%
102RT6.34 ± 0.719075 ± 1110
134+194RT5.68 ± 1.9185150 ± 4015
292RT276 ± 15722726 ± 38028
353RT130 ± 31282350 ± 28072
464RT221 ± 25202750 ± 36080
292170°C98 ± 758782 ± 4242
353170°C85 ± 1820828 ± 4080
464170°C55 ± 10071920 ±21093

The fitting parameters from the analysis of the LM-OSL curve using both general order and OTOR analytical equations_ The values are the mean between of the values obtained by the two different equations_ Error values provide a strong indication towards the agreement of the two different Equations used_

ComponentOSL Ttm (s)τ (s)Rb%
C1RT5.38 ± 0.450.036 ± 0.0030.61.72 ± 0.15
C2RT15.64 ± 0.220.306 ± 0.0030.71.823.3 ± 1.1
C3RT55.9 ± 4.13.9 ± 0.0030.831.935.5 ± 4
C4RT248 ± 3876.9 ± 0.0030.931.831.9 ± 2.9
C5RT1151 ± 4501667 ± 0.0030.011.17.29 ± 0.16
C1170°C4.33 ± 0.70.024 ± 0.0030.681.60.74 ± 0.18
C2170°C20.01 ± 0.400.506 ± 0.0030.831.6517.5 ± 1.3
C3170°C53 ± 0.53.51 ± 0.0030.811.816.4 ± 0.5
C4170°C244.8 ± 9.574.42 ± 0.0030.941.943.9 ± 2.1
C5170°C723 ± 92653 ± 0.0030.511.421.4 ± 2.5
Language: English
Page range: 222 - 231
Submitted on: Jan 15, 2019
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Accepted on: Oct 31, 2019
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Published on: Dec 31, 2021
Published by: Sciendo
In partnership with: Paradigm Publishing Services
Publication frequency: 1 issue per year

© 2021 Niyazi Meriç, Eren Şahiner, George Kitis, George S. Polymeris, published by Sciendo
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.