Automated Tobacco Investigation Using Flow-Injection Analysis (FIA) - AutomatisierteTabakuntersuchungmittelsFliessinjektionsanalyse (FlA)

Finster, P; Hollweg, J; Kausch, E; Burmester, U

doi:10.2478/cttr-2013-0590

Abstract

Watery tobacco extracts were examined with the aid of flow-injection analysis (FIA) for the substances nicotine, nitrate, chloride, ammonium and phosphate. The results proved to be exact and reproducible for the most part and the speed of analysis was between 37 and 113 measurements per hour. Because of its simple modular design the appliance is flexible in its application and is above all suited for the analysis for several components in small series of samples. A special FIA technique (stopped-flow method) enables the undersurface absorption stemming from the sample matrix to be excluded. The solutions used must exhibit uniform fluid composition and the formation of gas bubbles in the analysis system must be excluded.

References

1. Skeggs, L. T.: An automatic method for colorimet-ric analysis; Am. J. Clin. Pathol. 28 (1957) 311— 322.
Search in Google Scholar
2. Coakley, W. A.: Handbook of automated analysis — Continuous flow techniques; Marcel Dekker; Inc., New York, N.Y., und Basel, 1981.
Search in Google Scholar
3. Technicon Instruments Corporation, Tarrytown, N.Y.: Technicon Bibliography (AutoAnalyzer) 1957-1967/1968 und 1967—1973/1974.
Search in Google Scholar
4. Finster, P., F. Tödter und F. Seehofer: Automati-slerte Simultanbestimmung von Tabakinhaltsstof-fen (Teil I); LaborPraxis 6 (1982) 1362-1364.
Search in Google Scholar
5. Finster, P., F. Tödter und F. Seehofer: Automatic slerte Simultanbestimmung von Tabakinhaltsstof-fen (Teil II); LaborPraxis 8 (1984) 324-331.
Search in Google Scholar
6. Rüžčka, J., und E. H. Hansen: Flow injection analysis, Part I — A new concept of fast continuous flow analysis; Anal. Chim. Acta 78 (1975) 145-147.
Search in Google Scholar
7. Rüžčka, J., und E. H. Hansen: Flow injection analysis, Part X — Theory, techniques and trends; Anal. Chim. Acta 99 (1978) 37-76.
Search in Google Scholar
8. Rüžčka, J., und E. H. Hansen: Flow injection analysis — Principles, applications and trends; Anal. Chim. Acta 114 (1980) 19—44.
Search in Google Scholar
9. Möller, J.: FIA — Eine neue Analysenmethode; Prinzip und Möglicha;keiten der Flieβinjektionsanalyse; LaborPraxis 6 (1982) 278—296.
Search in Google Scholar
10. Karlberg, B., und J. Möller: Flow injection analysis — A new technique for the automation of wet-chemical procedures; In Focus 5 (1982) 5—11.
Search in Google Scholar
11. Möller, J.: FIA — Neue Techniken und Anwen-dungen; LaborPraxis 7 (1983) 162—168.
Search in Google Scholar
12. Müller, H., und V. Müllen Grundlagen und An-wendungen der Flow-injection-Analyse (FIA); Z. Chem. 24 (1984) 81—93.
Search in Google Scholar
13. Möller, J., und B. Winter: Application of flow injection techniques for the analysis of inorganic anions; Fresenius 2. Anal. Chem. 320 (1985) 451 — 456.
Search in Google Scholar
14. Dobbins, J. T., und J. M. Martin: Flow injection analysis — Twelve years old and growing; Spectroscopy 1 (1986) 20-29.
Search in Google Scholar
15. Hansen, E. H.: Recent advances in flow injection analysis; Int. Lab. 15, Nr. 8 (1985) 14-23.
Search in Google Scholar
16. a) Tecator AB (Höganäs, Schweden): FIAstar¯/ Flow injection analysis bibliography — Literature reference list with subject index and references/ 1974-1984, 135 S., 1985. b) Tecator AB (Höganäs, Schweden): FIAstar¯/ Flow injection analysis bibliography — Literature reference list with subject index and references / Supplement 1985, 81 S., 1986.
Search in Google Scholar
17. Mumpower, R. C., und G. T. Rasmussen: Automated measurement of smoke condensates; Proc. CORESTA 1982 Symposium, Wins ton-Salem, N.C., U.S.A., CORESTA Information Bulletin 1982, Special Issue, S. 17—18.
Search in Google Scholar
18. Davis, R. E.: The determination of nitrate in tobacco products using flow injection analysis; Vortrag anläβlich 38th Tobacco Chemists' Research Conference, Atlanta, Georgia, 1984.
Search in Google Scholar
19. Thomsen, H. V.: Flieβinjektionsanalyse; Vortrag anläβlich des XXV. Tabak-Kolloquiums, 1983, Delemont.
Search in Google Scholar
20. Burmester, U.: Einsata;zmöglichkeiten der Flieβ-In-jektions-Analyse zur Bestimmung von Tabakin-haltsstoffen; Diplomarbeh, Fachbereich Chemiein-genieurwesen, Fachhochschule Hamburg, 1986.
Search in Google Scholar
21. Finster, P., und J. Hollweg: Comparison of continuous flow and flow injection analysis methods for some tobacco constituents; Vortrag anläβlich der Tagung der Arbeitsgruppe Rauch der CORESTA in Bournemouth im September 1987.
Search in Google Scholar
22. Ranger, C. B.: Flow injection analysis — Principles, techniques, applications, design; Anal. Chem. 53 (1981) 20A-32A.
Search in Google Scholar
23. König, W.: Verfahren zur Darstellung neuer Stick-stoffhaltiger Farbstoffe; Z. Angew. Chem. 18 (1905) 115.
Search in Google Scholar
24. König, W.: Untersuchungen aus dem organischen Laboratorium der Technischen Hochschule zu Dresden — LXIX. Über eine neue, vom Pyridin derivierende Klasse von Farbstoffen; J, prakt. Chem. 69 (1904) 105—137.
Search in Google Scholar
25. Werle, E., und H. W. Becker: Über eine Mikrome-thode zur Bestimmung von Nicotin und ihre An-wendung zur Untersuchung der fermentativen Ni-cotinentgiftung durch tierisches Gewebe; Biochem. Z. 313 (1942) 182-191.
Search in Google Scholar
26. Sadler, W. W., R. R. Chesson und A. W. Schoen-baum: Automated procedure for determining the nicotine content of steam distillates; Tob. Sci. 4 (1960) 208—212.
Search in Google Scholar
27. DIN 10241: Tabak und Tabakerzeugnisse / Untersuchung — Bestimmung der Alkaloide in Tabaker-zeugnissen, Februar 1982.
Search in Google Scholar
28. Lidzey, R. G., und G. P. Savage: An automated procedure for the determination of total alkaloids in cigarette smoke using on-line cyanogen chloride generation from low hazard starting materials; Beitr. Tabakforsch. Int. 13 (1986) 151—155.
Search in Google Scholar
29. Saltzman, B. E.: Colorimetric microdetermination of nitrogen dioxide in the atmosphere; Anal. Chem, 26 (1954) 1949-1954.
Search in Google Scholar
30. Dölberg, U.; Über die Anwendung des Cadmium-Reduktors und der Diazotierung zur Bestimmung von Nitrat und Nitrit im Tabak; Beitr. Tabak-forsch. 3 (1965) 95-100,
Search in Google Scholar
31. Sloan, C. H., und B.J. Sublett: Colorimetric method of analysis for nitrates in tobacco; Tob. Sci. 10 (1966) 121-125.
Search in Google Scholar
32. Collins, P. F., J. F. Williams und B. H. Gerritsen: An automated method for the determination of nitrate in tobacco; Tob. Sci. 11 (1967) 75—78.
Search in Google Scholar
33. Tecator AB (Höganäs, Schweden): Determination of the sum of nitrate and nitrite in water by flow injection analysis; Tecator Application Note ASN 62-02/83, 1983.
Search in Google Scholar
34. Iwasaki, I., S. Utsumi und T. Ozawa: New colorimetric determination of chloride using mercuric thiocyanate and ferric ion; Bull. Chem. Soc. Jpn. 25 (1952) 226.
Search in Google Scholar
35. Iwasaki, I., S. Utsumi, K. Hagino und T. Ozawa: A new spectrophotometric method for the determination of small amounts of chloride using the mercuric thiocyanate method; Bull. Chem. Soc. Jpn. 29 (1956) 860-864.
Search in Google Scholar
36. Zall, D. M., D. Fisher und M. Q. Garner: Photometric determination of chlorides in water; Anal. Chem. 28 (1956) 1665—1668.
Search in Google Scholar
37. Rüžička, J., J. W. B. Stewart und E. A. Zagato: Flow injection analysis, Part IV — Stream sample splitting and its application to the continuous spectrophotometric determination of chloride in brackish waters; Anal. Chim. Acta 81 (1976) 387—396.
Search in Google Scholar
38. Van Son, M., R. C. Schothorst und G. den Boef: Determination of total ammoniacal nitrogen in water by flow injection analysis and a gas diffusion membrane (Short Communication); Anal. Chim. Acta 153 (1983) 271-275.
Search in Google Scholar
39. Lange, R., R. Friebe und F. Linow: Zur Anwendung der Methodenkombination Kjeldahl-Auf-schluβ / Berthelot-Reaktion bei der Stickstoffbe-stimmung in btologischen Materialien [1. Mitt.: Stand der Kenntnisse (Teil II)]; Nahrung 23 (1979) 431-439.
Search in Google Scholar
40. Ayers, C. W.: The determination of nitrogen and ammonia in tobacco and cigarette smoke; Proc. Soc, Analyt. Chem. 8 (1971) 17-19.
Search in Google Scholar
41. Collins, P. F., W. W. Lawrence und J. F. Williams: An automated procedure for the determination of ammonia in tobacco; Beitr. Tabakforsch. 6 (1972) 167-172.
Search in Google Scholar
42. Lange, B., und Z. J. Vejdfilek: Photometrische Analyse; Verlag Chemie, Weinheim, 1980.
Search in Google Scholar
43. Tecator AB (Höganas, Schweden): Determination of orthophosphate in water by flow injection analysis; Tecator Application Note ASN 60-02/83, 1983.
Search in Google Scholar
44. Rüžička, J., und E. H. Hansen: Flow injection analysis; John Wiley & Sons, New York, N.Y., 1981.
Search in Google Scholar
45. Kausch, E., H. Haffner und P. Finster: Die Anwendung enzymatischer Analysenmethoden in der Cigarettenindustrie; Vortrag anlä'βlich des XXIV. Tabak-Kolloquiums, Bad Harzburg, 1982.
Search in Google Scholar
46. Engelhardt, H., und R. Klinkner: Durchfluβanaly-tische Phosphatbestimmung unter Verwendung geometrisch verformter offener Rohren; Fresenius Z. Anal. Chem. 319 (1984) 277—281.
Search in Google Scholar
47. Rüžička, J.; und E. H. Hansen: Optosensing at active surfaces — A new detection principle in flow injection analysis; Anal. Chim. Acta 173 (1985) 3-21.
Search in Google Scholar
48. Schelter-Graf, A., H. Huck und H.-L. Schmidt: Rasche und genaue Bestimmung von Ethanol mit-tels einer Oxidase-Elektrode in einem Stromungs-Injektions-System; Z. Lebensm. Unters. Forsch. 177 (1983) 356-358.
Search in Google Scholar
49. Hansen, E. H., A. Chose and J. Rüžička: Flow injection analysis of environmental samples for nitrate using an ion-selective electrode; Analyst 102 (1977) 705—713.
Search in Google Scholar
50. Mutler, H., und G. Wallaschek: Wasserbestimmun-gen in organischen Lösungsmitteln nach der Karl-Fischer-Methode unter Flow-injection-Bedingun-gen; Z. Chem. 24 (1984) 75-76.
Search in Google Scholar

Automated Tobacco Investigation Using Flow-Injection Analysis (FIA) - AutomatisierteTabakuntersuchungmittelsFliessinjektionsanalyse (FlA)

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