Gas Chromatographic Analysis of Cigarette Smoke by Trimethylsilylation Method

S. Ishiguro; S. Sugawara

doi:10.2478/cttr-2013-0451

.blurhash-client-img { display: none !important; }

Gas Chromatographic Analysis of Cigarette Smoke by Trimethylsilylation Method

Contributions to Tobacco & Nicotine Research

Volume 9 (1978): Issue 4 (July 1978)

By: S. Ishiguro and S. Sugawara

Open Access

|Aug 2014

Abstract

A gas chromatographic method was developed to quantitatively determine the major components in the total particulate matter (TPM) of cigarette smoke. Tobacco smoke condensate was collected on a glass fiber filter and the components were converted to their trimethylsilyl derivatives and then subjected to glass capillary column gas chromatography. By this method, volatile and non-volatile tobacco smoke components, including unstable phenolic substances and water-soluble polyhydroxy compounds, were determined simultaneously

References

1. Stedman, R. L.: Chem. Rev. 68 (i968) 153.10.1021/cr60252a002
Search in Google Scholar
2. Neurath, G.: Beitr. Tabakforsch. 5 (1969) 115.
Search in Google Scholar
3. Johnson, W. R., R. W. Hale and J. W. Nedlock: Tob. Sci. 17 (1973) 73.
Search in Google Scholar
4. Kaburaki, Y., H. Shigematsu, Y. Yamashita and H. Kusakabe: Agric. Bioi. Chem. 35 (1971) 1741. 5, Shigematsu, H., R. Ono, Y. Yamashita and Y. Kaburaki: ibid. 35 (1971) 1751.
Search in Google Scholar
6. Ishiguro, S., S. Sato, S. Sugawara and Y. Kaburaki: ibid. 40 (1976) 977.
Search in Google Scholar
7. Ishiguro, S., S. Yano, S. Sugawara and Y. Kaburaki: ibid. 40 (1976) 2005.
Search in Google Scholar
8. Ishiguro, S., and S. Sugawara: ibid. 41 (1977) 377.
Search in Google Scholar
9. Schumacher, J. N., C. R. Green, F. W. Best and M. P. Newell: J. Agric. Food Chem. 25 (1977) 310.10.1021/jf60210a003
Search in Google Scholar
10. Grob, K.: Beitr. Tabakforsch. 5 (1969) 52.
Search in Google Scholar
11. Grob., K.: J. Gas Chromatog. 3 (1965) 52.10.1093/chromsci/3.2.52
Search in Google Scholar
12. Guerin, M. R., and G. Olerich: Tob. Sci. 20 (1976) 19.
Search in Google Scholar
13. Guerin, M. R., G. Olerich and A. D. Horton: J. Chrom. Sci. 12 (1974) 385.10.1093/chromsci/12.7.385
Search in Google Scholar
14. Rowland, R. L.: J. Amer. Chem. Soc. 79 (1957) 5007.10.1021/ja01575a048
Search in Google Scholar
15. Zane, A., and S. H. Wender: Tob. Sci. 7 (1963) 21.
Search in Google Scholar
16. Leach, J. T., E. D. Alford and E. F. Litzinger: ibid. 13 (1969) 53.
Search in Google Scholar
17. Chuman, T., and M. Noguchi: Agric. Bioi. Chem. 41 (1977) 1021.10.1080/00021369.1977.10862608
Search in Google Scholar
18. Gardiner, D.: J. Chem. Soc. London (Sect. C) 1966, 1473.10.1039/j39660001473
Search in Google Scholar
19. Sakuma, H., M. Kusama, S. Sato and S. Sugawara: Agric. Biol. Chem. 40 (1976) 2013.
Search in Google Scholar
20. Sakuma, H., M. Kusama, S. Ishiguro, N. Shimojima and S. Sugawara: ibid. 40 (1976) 2021.
Search in Google Scholar
21. Nakagawa, Y., C. H. Yang and S. H. Wender: J, Org. Chem. 26 (1961) 3017.10.1021/jo01066a627
Search in Google Scholar
22. Shigematsu, H., S. Shibata, T. Kurata, H. Kato and M. Fujimaki: J. Agric. Food Chem. 23 (1975) 233.10.1021/jf60198a033
Search in Google Scholar
23. Veahear, L. A. T., and H. G. J. Wilt: J. Chromatog. 41 (1969) 168.10.1016/0021-9673(64)80120-5
Search in Google Scholar

Articles in this issue

DOI: https://doi.org/10.2478/cttr-2013-0451 | Journal eISSN: 2719-9509

Journal RSS Feed

Language: English

Page range: 218 - 221

Published on: Aug 14, 2014

Published by: Institut für Tabakforschung GmbH

In partnership with: Paradigm Publishing Services

Publication frequency: 4 issues per year

Related subjects:

General interest,

Life sciences,

Life sciences, other,

Physics,

Physics, other

© 2014 S. Ishiguro, S. Sugawara, published by Institut für Tabakforschung GmbH
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Volume 9 (1978): Issue 4 (July 1978)