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PbS nanopowder – synthesis, characterization and antimicrobial activity Cover

PbS nanopowder – synthesis, characterization and antimicrobial activity

By: M. Suganya and  A.R. Balu  
Open Access
|Jul 2017

Abstract

Lead sulphide (PbS) nanopowder was synthesized by a simple soft chemical route using lead nitrate and thiourea as precursor salts. The as-synthesized nanopowder was characterized by XRD, SEM, EDX, FT-IR, PL, Raman and magnetic measurements. XRD studies reveal the polycrystalline nature of the powder. The powder exhibits face-centered cubic structure with a strong (2 0 0) preferential orientation. The presence of Pb and S in the powder is confirmed by energy dispersive X-ray analysis. The peaks observed at 1112 cm-1 and at 606 cm-1 in the FT-IR spectrum are related to heteropolar diatomic molecules of PbS. The Raman peak shift at 173 cm-1 might have originated from the combination of longitudinal and transverse acoustic phonon modes associated with PbS crystal. The M-H loop confirms the paramagnetic nature of the as-synthesized PbS nanopowder. The nanopowder has significant antimicrobial activity against certain bacteria and fungi strains which make it suitable as antimicrobial agent against pathogenic microorganisms.

DOI: https://doi.org/10.1515/msp-2017-0046 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
Language: English
Page range: 322 - 328
Submitted on: Jul 3, 2016
Accepted on: Mar 19, 2017
Published on: Jul 26, 2017
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year

© 2017 M. Suganya, A.R. Balu, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.