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One step paired electrochemical synthesis of iron and iron oxide nanoparticles

Materials Science-Poland
Volume 34 (2016): Issue 3 (September 2016)
By:
Open Access
|Sep 2016

Figures & Tables

Fig. 1

SEM images of synthesized nanoparticles: (a) iron, (b) iron oxide, and TEM images: (c) iron, (d) iron oxide.
SEM images of synthesized nanoparticles: (a) iron, (b) iron oxide, and TEM images: (c) iron, (d) iron oxide.

Fig. 2

FT-IR spectra of synthesized nanoparticles: (a) goethite and (b) hematite.
FT-IR spectra of synthesized nanoparticles: (a) goethite and (b) hematite.

Fig. 3

XRD patterns of synthesized nanoparticles: (a) iron and (b) iron oxide.
XRD patterns of synthesized nanoparticles: (a) iron and (b) iron oxide.

Fig. 4

Magnetization curves of synthesized nanoparticles: (a) iron and (b) iron oxide.
Magnetization curves of synthesized nanoparticles: (a) iron and (b) iron oxide.

Comparison of VSM results of synthesized nanoparticles with published data_

NanoparticleMorphologySize[nm]Ms[emu × g-1]Reference
Ironcoreshell<44132[18]
1060
spherical30130This work
Hematitesubrounded8772[19]
368.6
spherical7075This work
DOI: https://doi.org/10.1515/msp-2016-0090 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 655 - 658
Submitted on: Jan 21, 2016
Accepted on: Jul 15, 2016
Published on: Sep 12, 2016
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 times per year
Keywords:
nanoparticles,
electrodeposition,
pulsed current method,
paired electrosynthesis,
magnetic materials
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2016 Juliet Ordoukhanian, Hassan Karami, Azizollah Nezhadali, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.

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