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Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method Cover

Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method

Materials Science-Poland
Volume 34 (2016): Issue 3 (September 2016)
By:  and    
Open Access
|Sep 2016
Figures & tables

Figures & Tables

Fig. 1

XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 2

TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 3

EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 4

Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.

Effects of the experimental conditions on the structure of the CdS nanoparticles_

SampleKind of methodCompositionReaction timeStructure
S1sonochemicalCd(NO3)2 + TAA (1:2)40 mincubic
S2sonochemicalCd(NO3)2 + Na2S (1:2)40 mincubic
S3combined sonochemical-solvothermalCd(NO3)2+ TAA (1:2)40 minhexagonal (irregular)
S4combined sonochemical-solvothermalCd(NO3)2+ TAA (1:4)1 hhexagonal (irregular)
S5combined sonochemical-solvothermalCd(NO3 )2 + Na2S(1:4)1 hhexagonal (irregular)
S6combined sonochemical-solvothermalCd(NO3)2 + Na2S (1:4)5 hhexagonal
DOI: https://doi.org/10.1515/msp-2016-0089 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 684 - 690
Submitted on: Apr 4, 2016
Accepted on: Jul 11, 2016
Published on: Sep 28, 2016
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 issues per year
Keywords:
nanorods,
semiconductor,
sonochemical-solvothermal method,
characterization
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2016 Pinar Acar Bozkurt, Burak Derkuş, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.

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