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Synthesis and characterization of CdS nanorods by combined sonochemical-solvothermal method

Materials Science-Poland
Volume 34 (2016): Issue 3 (September 2016)
By:
Open Access
|Sep 2016

Figures & Tables

Fig. 1

XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
XRD patterns of CdS nanoparticles synthesized by different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 2

TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
TEM images of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 3

EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).
EDX spectrum of CdS nanoparticles synthesized with different methods (a) sonochemical method (Sample S1), (b) combined sonochemical-solvothermal method (Sample S6).

Fig. 4

Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.
Schematic presentation and structural development of synthesized CdS nanoparticles obtained using different experimental procedures.

Effects of the experimental conditions on the structure of the CdS nanoparticles_

SampleKind of methodCompositionReaction timeStructure
S1sonochemicalCd(NO3)2 + TAA (1:2)40 mincubic
S2sonochemicalCd(NO3)2 + Na2S (1:2)40 mincubic
S3combined sonochemical-solvothermalCd(NO3)2+ TAA (1:2)40 minhexagonal (irregular)
S4combined sonochemical-solvothermalCd(NO3)2+ TAA (1:4)1 hhexagonal (irregular)
S5combined sonochemical-solvothermalCd(NO3 )2 + Na2S(1:4)1 hhexagonal (irregular)
S6combined sonochemical-solvothermalCd(NO3)2 + Na2S (1:4)5 hhexagonal
DOI: https://doi.org/10.1515/msp-2016-0089 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 684 - 690
Submitted on: Apr 4, 2016
Accepted on: Jul 11, 2016
Published on: Sep 28, 2016
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 times per year
Keywords:
nanorods,
semiconductor,
sonochemical-solvothermal method,
characterization
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2016 Pinar Acar Bozkurt, Burak Derkuş, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.

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