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Synthesis and 3D-AFM surface topology of nanographene-like material extracted from sulfonated tri-, di- and monochloroacetic acid

Materials Science-Poland
Volume 34 (2016): Issue 3 (September 2016)
By:
Open Access
|Sep 2016

Figures & Tables

Fig. 1

Gray color gradient for graphite dispersed in different substituted chloroacetic acids: (a) trichloroacetic acid, (b) dichloroacetic acid, (c) monochloroacetic acid.
Gray color gradient for graphite dispersed in different substituted chloroacetic acids: (a) trichloroacetic acid, (b) dichloroacetic acid, (c) monochloroacetic acid.

Fig. 2

(a) Raman spectrum measured for ground graphene flakes, (b) X-ray diffraction pattern recorded for graphene-like material flakes, (c) high-resolution XRD pattern at very narrow 2θ range recorded for graphene-like material dispersed in tricholoroacetic acid as a solvent.
(a) Raman spectrum measured for ground graphene flakes, (b) X-ray diffraction pattern recorded for graphene-like material flakes, (c) high-resolution XRD pattern at very narrow 2θ range recorded for graphene-like material dispersed in tricholoroacetic acid as a solvent.

Fig. 3

(a) 3D-image for graphene-like material in tapping non-contact mode, (b) 2D-AFM image for graphene-like material in tapping non-contact mode, (c) honeycomb structure of graphene.
(a) 3D-image for graphene-like material in tapping non-contact mode, (b) 2D-AFM image for graphene-like material in tapping non-contact mode, (c) honeycomb structure of graphene.

Fig. 4

3D-AFM-visualized image for the synthesized graphene-like material.
3D-AFM-visualized image for the synthesized graphene-like material.

Fig. 5

Histogram of x-z axes of graphene-like material.
Histogram of x-z axes of graphene-like material.
DOI: https://doi.org/10.1515/msp-2016-0081 | Journal eISSN: 2083-134X | Journal ISSN: 2083-1331
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Language: English
Page range: 627 - 632
Submitted on: Jan 8, 2016
Accepted on: Jun 29, 2016
Published on: Sep 21, 2016
Published by: Wroclaw University of Science and Technology
In partnership with: Paradigm Publishing Services
Publication frequency: 4 times per year
Keywords:
synthesis,
dispersion,
AFM,
graphene,
Raman spectra
Related subjects:
Materials sciences,
Materials sciences, other,
Nanomaterials,
Functional and smart materials,
Materials characterization and properties

© 2016 Khaled M. Elsabawy, published by Wroclaw University of Science and Technology
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.

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