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Acid etching behavior and mechanism in acid solution of iron components in basalt fibers Cover

Acid etching behavior and mechanism in acid solution of iron components in basalt fibers

Open Access
|Sep 2025

Figures & Tables

Figure 1

Standard curve of iron.
Standard curve of iron.

Figure 2

Relationship between acid-etching time and dissolution rate of iron components.
Relationship between acid-etching time and dissolution rate of iron components.

Figure 3

Relationship between sulfuric acid concentration and dissolution rate of iron components.
Relationship between sulfuric acid concentration and dissolution rate of iron components.

Figure 4

Relationship between temperature and dissolution rate of iron components.
Relationship between temperature and dissolution rate of iron components.

Figure 5

Relationship between liquid–solid ratio and dissolution rate of iron components.
Relationship between liquid–solid ratio and dissolution rate of iron components.

Figure 6

XRD patterns of basalt fibers before and after acid etching.
XRD patterns of basalt fibers before and after acid etching.

Figure 7

Morphological changes and micro-analysis results of basalt fiber before and after acid etching before acid etching, (b) after acid etching, (c) micro-analysis result of basalt fiber before acid etching, (d) micro-analysis result of basalt fiber after acid etching.
Morphological changes and micro-analysis results of basalt fiber before and after acid etching before acid etching, (b) after acid etching, (c) micro-analysis result of basalt fiber before acid etching, (d) micro-analysis result of basalt fiber after acid etching.

Figure 8

XPS analysis results of basalt fiber before (a) and after (b) acid etching.
XPS analysis results of basalt fiber before (a) and after (b) acid etching.

Figure 9

Mechanism diagram of the iron component in basalt fiber in sulfuric acid solution.
Mechanism diagram of the iron component in basalt fiber in sulfuric acid solution.

Dissolution of iron components in basalt fiber

NumberDissolution ratio (%)Total iron content (mg)Ferrous iron content (mg)
BFSL-Y-011.727.31121.0875
BFSL-Y-021.597.32680.9458
BFSL-Y-031.677.30340.9551
Average value1.667.31380.9961
R 2 2.38%0.02%7.99%

Acid etching experimental scheme of iron components in basalt fiber

Leaching time (h)Sulfuric acid concentration (mol/L)Temperature (°C)Liquid–solid ratio (mL/g)
Scheme12, 4, 6, 8, 1018020:1
Scheme241, 2, 3, 4, 58020:1
Scheme34150, 60, 70, 90, 10020:1
Scheme4419010:1, 15:1, 20:1, 25:1, 30:1

Main chemical composition of basalt fiber

CompositionSiO2 CaOAl2O3 Fe2O3 MgOTiO2 Na2OK2O
Content/%50.639.3214.3811.208.321.333.740.61
Language: English
Submitted on: Oct 8, 2024
Accepted on: Jul 2, 2025
Published on: Sep 18, 2025
Published by: Sciendo
In partnership with: Paradigm Publishing Services

© 2025 Lvshan Zhou, Jingfan Xu, Zhenxiao Deng, Yunfei Zhang, published by Sciendo
This work is licensed under the Creative Commons Attribution 4.0 License.