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The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives

Open Access
|Jun 2016

Abstract

Zeolite Y clay modified copper nitrate catalyst was prepared. The obtained catalyst was analyzed by SEM, EDS, and powder XRD techniques. The zeolite Y clay modified copper nitrate catalyst was used for the synthesis of various substituted mesalazine by sulfonylation. The synthesized sulfonamides have been characterized by GC-MS, IR, 1H, 13C and HSQC NMR techniques. The yield percentages of sulfonamides are more than 85%.

DOI: https://doi.org/10.1515/auoc-2016-0005 | Journal eISSN: 2286-038X | Journal ISSN: 1583-2430
Language: English
Page range: 22 - 27
Submitted on: Mar 17, 2016
Accepted on: May 6, 2016
Published on: Jun 28, 2016
Published by: Ovidius University of Constanta
In partnership with: Paradigm Publishing Services
Publication frequency: 2 times per year
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© 2016 Selvakumar Dineshkumar, Ganesamoorthi Thirunarayanan, Perumal Mayavel, Inbasekaran Muthuvel, published by Ovidius University of Constanta
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.