The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives

Selvakumar Dineshkumar; Ganesamoorthi Thirunarayanan; Perumal Mayavel; Inbasekaran Muthuvel

doi:10.1515/auoc-2016-0005

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The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives

Ovidius University Annals of Chemistry

Volume 27 (2016): Issue 1 (June 2016)

By: Selvakumar Dineshkumar, Ganesamoorthi Thirunarayanan, Perumal Mayavel and Inbasekaran Muthuvel

Open Access

|Jun 2016

Abstract

Zeolite Y clay modified copper nitrate catalyst was prepared. The obtained catalyst was analyzed by SEM, EDS, and powder XRD techniques. The zeolite Y clay modified copper nitrate catalyst was used for the synthesis of various substituted mesalazine by sulfonylation. The synthesized sulfonamides have been characterized by GC-MS, IR, ¹H, ¹³C and HSQC NMR techniques. The yield percentages of sulfonamides are more than 85%.

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Articles in this issue

DOI: https://doi.org/10.1515/auoc-2016-0005 | Journal eISSN: 2286-038X | Journal ISSN: 1583-2430

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Language: English

Page range: 22 - 27

Submitted on: Mar 17, 2016

Accepted on: May 6, 2016

Published on: Jun 28, 2016

Published by: Ovidius University of Constanta

In partnership with: Paradigm Publishing Services

Publication frequency: 2 issues per year

Keywords:

sulfonamides,

copper-zeolites,

FT-IR,

NMR spectra,

GC-mass,

SEM,

EDS,

powder XRD

Related subjects:

Chemistry,

Chemistry, other

© 2016 Selvakumar Dineshkumar, Ganesamoorthi Thirunarayanan, Perumal Mayavel, Inbasekaran Muthuvel, published by Ovidius University of Constanta
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.

Volume 27 (2016): Issue 1 (June 2016)